C₈₀H₈₀N₂O₄

Base Information

• Chemical Name: C₈₀H₈₀N₂O₄
• CAS No.: 1335223-99-8
• Molecular Formula: C₈₀H₈₀N₂O₄
• Molecular Weight: 1133.53
• Mol file: 1335223-99-8.mol

Synonyms:C₈₀H₈₀N₂O₄

Chemical Property of C₈₀H₈₀N₂O₄

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₈₀H₈₀N₂O₄

There total 5 articles about C₈₀H₈₀N₂O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

C40H41NO2 (1335223-98-7) → C80H80N2O4 (1335223-99-8)

Guidance literature:

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; scandium tris(trifluoromethanesulfonate); In dichloromethane; at 25 ℃; for 0.166667h; Inert atmosphere;

DOI:10.1039/c1cc13398e

Reference yield:

1-dodecylbromide (143-15-7) → C80H80N2O4 (1335223-99-8)

Guidance literature:

Multi-step reaction with 4 steps

1: sodium hydride / tetrahydrofuran / 12 h / 66 °C / Inert atmosphere

2: N-Bromosuccinimide / N,N-dimethyl-formamide / 2 h / 25 °C

3: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / tetrahydrofuran; water / 12 h / 66 °C / Inert atmosphere

4: 2,3-dicyano-5,6-dichloro-p-benzoquinone; scandium tris(trifluoromethanesulfonate) / dichloromethane / 0.17 h / 25 °C / Inert atmosphere

With N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium hydride; potassium carbonate; 2,3-dicyano-5,6-dichloro-p-benzoquinone; scandium tris(trifluoromethanesulfonate); In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; 3: Suzuki-Miyaura coupling;

DOI:10.1039/c1cc13398e

Reference yield:

1-hydrophenanthrene[1,10,9,8-cdefg]carbazole (35337-22-5) → C80H80N2O4 (1335223-99-8)

Guidance literature:

Multi-step reaction with 4 steps

1: sodium hydride / tetrahydrofuran / 12 h / 66 °C / Inert atmosphere

2: N-Bromosuccinimide / N,N-dimethyl-formamide / 2 h / 25 °C

3: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / tetrahydrofuran; water / 12 h / 66 °C / Inert atmosphere

4: 2,3-dicyano-5,6-dichloro-p-benzoquinone; scandium tris(trifluoromethanesulfonate) / dichloromethane / 0.17 h / 25 °C / Inert atmosphere

With N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium hydride; potassium carbonate; 2,3-dicyano-5,6-dichloro-p-benzoquinone; scandium tris(trifluoromethanesulfonate); In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; 3: Suzuki-Miyaura coupling;

DOI:10.1039/c1cc13398e

upstream raw materials:

1-hydrophenanthrene[1,10,9,8-cdefg]carbazole

1-dodecyl-1H-phenanthro[1,10,9,8-c,d,e,f,g]carbazole

C₃₂H₃₄BrN

C₄₀H₄₁NO₂

Downstream raw materials:

C₇₈H₇₆N₂O₄

C₁₂₆H₁₇₂N₂O₄