8-<(4-methoxyphenyl)methoxy>-3-<(methoxycarbonyl)oxy>-2-<(trimethylsilyl)methyl>-1-octene

Base Information

Chemical Name:8-<(4-methoxyphenyl)methoxy>-3-<(methoxycarbonyl)oxy>-2-<(trimethylsilyl)methyl>-1-octene
CAS No.:136276-88-5
Molecular Formula:C₂₂H₃₆O₅Si
Molecular Weight:408.61
Hs Code.:

Synonyms:8-<(4-methoxyphenyl)methoxy>-3-<(methoxycarbonyl)oxy>-2-<(trimethylsilyl)methyl>-1-octene

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Chemical Property of 8-<(4-methoxyphenyl)methoxy>-3-<(methoxycarbonyl)oxy>-2-<(trimethylsilyl)methyl>-1-octene

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Technology Process of 8-<(4-methoxyphenyl)methoxy>-3-<(methoxycarbonyl)oxy>-2-<(trimethylsilyl)methyl>-1-octene

There total 4 articles about 8-<(4-methoxyphenyl)methoxy>-3-<(methoxycarbonyl)oxy>-2-<(trimethylsilyl)methyl>-1-octene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 629-11-8
1,6-hexanediol

: 136276-88-5
8-<(4-methoxyphenyl)methoxy>-3-<(methoxycarbonyl)oxy>-2-<(trimethylsilyl)methyl>-1-octene

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) potassium hydride, 2.) tetrabutylammonium iodide / 1.) hexane, THF, from 0 deg C to RT, 40 min, 2.) hexane, THF, overnight

2: 72 percent / pyridinium chlorochromate (PCC), Celite / CH₂Cl₂ / 1.5 h / Ambient temperature

With Celite; tetra-(n-butyl)ammonium iodide; potassium hydride; pyridinium chlorochromate; In dichloromethane;
DOI:10.1021/ja00019a036

Reference yield:

: 2746-25-0
p-Methoxybenzyl bromide

: 136276-88-5
8-<(4-methoxyphenyl)methoxy>-3-<(methoxycarbonyl)oxy>-2-<(trimethylsilyl)methyl>-1-octene

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) potassium hydride, 2.) tetrabutylammonium iodide / 1.) hexane, THF, from 0 deg C to RT, 40 min, 2.) hexane, THF, overnight

2: 72 percent / pyridinium chlorochromate (PCC), Celite / CH₂Cl₂ / 1.5 h / Ambient temperature

With Celite; tetra-(n-butyl)ammonium iodide; potassium hydride; pyridinium chlorochromate; In dichloromethane;
DOI:10.1021/ja00019a036

Reference yield:

: 105192-33-4
6-<(4-methoxyphenyl)methoxy>hexan-1-ol

: 136276-88-5
8-<(4-methoxyphenyl)methoxy>-3-<(methoxycarbonyl)oxy>-2-<(trimethylsilyl)methyl>-1-octene

Guidance literature:: Multi-step reaction with 2 steps

1: 72 percent / pyridinium chlorochromate (PCC), Celite / CH₂Cl₂ / 1.5 h / Ambient temperature

With Celite; pyridinium chlorochromate; In dichloromethane;
DOI:10.1021/ja00019a036