Technology Process of C31H27BrN2O2
There total 3 articles about C31H27BrN2O2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
1,8-diazabicyclo[5.4.0]undec-7-ene; 1,4-dimethyl-1,2,4-triazolium iodide;
In
methanol;
at 0 ℃;
for 0.5h;
Reagent/catalyst;
Temperature;
Time;
Molecular sieve;
DOI:10.1002/anie.201208349
- Guidance literature:
-
4-phenyl-hexa-2,4-dienal; C18H11BrN2;
With
C44H77NO4Si2; salicylic acid;
In
1,4-dioxane;
at 50 ℃;
for 12h;
With
1,8-diazabicyclo[5.4.0]undec-7-ene; 1,4-dimethyl-1,2,4-triazolium iodide;
In
1,4-dioxane; methanol;
at 0 ℃;
for 0.5h;
Reagent/catalyst;
Solvent;
Temperature;
Time;
Molecular sieve;
DOI:10.1002/anie.201208349
- Guidance literature:
-
4-phenyl-hexa-2,4-dienal; C12H7BrN2;
With
C44H77NO4Si2; salicylic acid;
In
1,4-dioxane;
at 50 ℃;
for 12h;
With
1,8-diazabicyclo[5.4.0]undec-7-ene; 1,4-dimethyl-1,2,4-triazolium iodide;
In
1,4-dioxane; methanol;
at 0 ℃;
for 0.5h;
Reagent/catalyst;
Solvent;
Temperature;
Time;
enantioselective reaction;
Molecular sieve;
DOI:10.1002/anie.201208349