Ph₃SiGePh₂GePh₃

Base Information

Chemical Name:Ph₃SiGePh₂GePh₃
CAS No.:149033-89-6
Molecular Formula:C₄₈H₄₀Ge₂Si
Molecular Weight:790.111
Hs Code.:

Ph<sub>3</sub>SiGePh<sub>2</sub>GePh<sub>3</sub>

Synonyms:Ph₃SiGePh₂GePh₃

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Chemical Property of Ph₃SiGePh₂GePh₃

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Technology Process of Ph₃SiGePh₂GePh₃

There total 3 articles about Ph₃SiGePh₂GePh₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 18.0%

: 149033-91-0
ClPh₂GeSiPh₃

: 57482-41-4
Triphenylgermyl-kalium

: 149033-89-6
Ph₃SiGePh₂GePh₃

Guidance literature:: With Na₂SO₄; HCl; In diethyl ether; addn. of KGe(C6H5)3 in ether to a solution of the silyl germane at -78 ° C within 30 min; stirring for 2 h; the mixture was allowed to warm to room temperature; addn. of 1 N HCl;; filtration; the ether layer was dried over Na2SO4; solvent removal; recrystn. from toluene/heptane; elem. anal.;;
DOI:10.1016/0022-328X(93)80184-D

Reference yield:

: 2816-39-9
hexaphenyldigermane

: 149033-89-6
Ph₃SiGePh₂GePh₃

Guidance literature:: Multi-step reaction with 2 steps

1: diethyl ether; tetrahydrofuran

2: Na₂SO₄; HCl / diethyl ether

With Na₂SO₄; HCl; In tetrahydrofuran; diethyl ether;
DOI:10.1016/0022-328X(93)80184-D

Reference yield:

: 15487-82-8,6735-25-7
triphenylsilylkalium

: 1613-66-7
dichlorodiphenylgermane

: 149033-89-6
Ph₃SiGePh₂GePh₃

Guidance literature:: Multi-step reaction with 2 steps

1: HCl / diethyl ether

2: Na₂SO₄; HCl / diethyl ether

With HCl; Na₂SO₄; In diethyl ether;
DOI:10.1016/0022-328X(93)80184-D