5-O-benzyl-1,2-O-cyclohexylidene-3-deoxy-2-C-methyl-β-D-threo-pentofuranose

Base Information

Chemical Name:5-O-benzyl-1,2-O-cyclohexylidene-3-deoxy-2-C-methyl-β-D-threo-pentofuranose
CAS No.:62053-94-5
Molecular Formula:C₁₉H₂₆O₄
Molecular Weight:318.413
Hs Code.:

Synonyms:5-O-benzyl-1,2-O-cyclohexylidene-3-deoxy-2-C-methyl-β-D-threo-pentofuranose

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Chemical Property of 5-O-benzyl-1,2-O-cyclohexylidene-3-deoxy-2-C-methyl-β-D-threo-pentofuranose

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Technology Process of 5-O-benzyl-1,2-O-cyclohexylidene-3-deoxy-2-C-methyl-β-D-threo-pentofuranose

There total 4 articles about 5-O-benzyl-1,2-O-cyclohexylidene-3-deoxy-2-C-methyl-β-D-threo-pentofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 86883-26-3
methyl 5-O-benzyl-3-deoxy-2-C-methyl-β-D-threo-pentofuranoside

: 62053-94-5
5-O-benzyl-1,2-O-cyclohexylidene-3-deoxy-2-C-methyl-β-D-threo-pentofuranose

Guidance literature:: With sulfuric acid; In benzene; for 0.5h; Ambient temperature;
DOI:10.1246/bcsj.56.1095

Reference yield:

: 67737-48-8
methyl 5-benzyloxy-β-D-ribofuranoside

: 62053-94-5
5-O-benzyl-1,2-O-cyclohexylidene-3-deoxy-2-C-methyl-β-D-threo-pentofuranose

Guidance literature:: Multi-step reaction with 3 steps

1: 52 percent / pyridine / 0 - 5 °C

2: 81 percent / diethyl ether; benzene / 2 h / Ambient temperature

3: 59 percent / concd. H₂SO₄ / benzene / 0.5 h / Ambient temperature

With pyridine; sulfuric acid; In diethyl ether; benzene;
DOI:10.1246/bcsj.56.1095

Reference yield:

: 86861-81-6
Toluene-4-sulfonic acid (2R,3S,4R,5R)-2-benzyloxymethyl-4-hydroxy-5-methoxy-tetrahydro-furan-3-yl ester

: 62053-94-5
5-O-benzyl-1,2-O-cyclohexylidene-3-deoxy-2-C-methyl-β-D-threo-pentofuranose

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / diethyl ether; benzene / 2 h / Ambient temperature

2: 59 percent / concd. H₂SO₄ / benzene / 0.5 h / Ambient temperature

With sulfuric acid; In diethyl ether; benzene;
DOI:10.1246/bcsj.56.1095