Technology Process of (E)-butyl 3-(5-methyl-2-(pyridin-2-ylsulfinyl)phenyl)acrylate
There total 4 articles about (E)-butyl 3-(5-methyl-2-(pyridin-2-ylsulfinyl)phenyl)acrylate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
dipotassium peroxodisulfate; palladium diacetate;
In
1,2-dichloro-ethane;
at 110 ℃;
for 20h;
Inert atmosphere;
DOI:10.1002/chem.201003633
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 - 20 °C / Inert atmosphere
2: dipotassium peroxodisulfate; palladium diacetate / 1,2-dichloro-ethane / 20 h / 110 °C / Inert atmosphere
With
dipotassium peroxodisulfate; palladium diacetate; 3-chloro-benzenecarboperoxoic acid;
In
dichloromethane; 1,2-dichloro-ethane;
DOI:10.1002/chem.201003633
- Guidance literature:
-
Multi-step reaction with 3 steps
1: potassium carbonate / dimethyl sulfoxide / 18 h / 110 °C / Inert atmosphere
2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 - 20 °C / Inert atmosphere
3: dipotassium peroxodisulfate; palladium diacetate / 1,2-dichloro-ethane / 20 h / 110 °C / Inert atmosphere
With
dipotassium peroxodisulfate; palladium diacetate; potassium carbonate; 3-chloro-benzenecarboperoxoic acid;
In
dichloromethane; dimethyl sulfoxide; 1,2-dichloro-ethane;
DOI:10.1002/chem.201003633
