Ph₂Ge(Cl)CH₂CH₂OEt

Base Information

Chemical Name:Ph₂Ge(Cl)CH₂CH₂OEt
CAS No.:894804-34-3
Molecular Formula:C₁₆H₁₉ClGeO
Molecular Weight:335.369
Hs Code.:

Ph<sub>2</sub>Ge(Cl)CH<sub>2</sub>CH<sub>2</sub>OEt

Synonyms:Ph₂Ge(Cl)CH₂CH₂OEt

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Chemical Property of Ph₂Ge(Cl)CH₂CH₂OEt

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Technology Process of Ph₂Ge(Cl)CH₂CH₂OEt

There total 1 articles about Ph₂Ge(Cl)CH₂CH₂OEt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 7366-23-6
diphenylchlorogermane

: 109-92-2,25104-37-4
ethyl vinyl ether

: 894804-34-3
Ph₂Ge(Cl)CH₂CH₂OEt

Guidance literature:: With AIBN; In benzene; High Pressure; under inert atm. to soln. Ph2GeHCl in benzene ethyl vinyl ether was added, soln. AIBN in benzene was added, and heated in tube sealed with Teflon plug at 85°C for 24 h; volatiles were removed in vacuo; elem. anal.;
DOI:10.1021/om060115x

Reference yield: 86.0%

: 894804-34-3
Ph₂Ge(Cl)CH₂CH₂OEt

: 3585-33-9
lithium dimethylamide

: 894804-38-7
Ph₂Ge(NMe₂)CH₂CH₂OEt

Guidance literature:: In benzene; byproducts: LiCl; under inert atm. to soln. Ph2Ge(Cl)CH2CH2OEt in benzene LiNMe2 was addedand stirred at room temp. for 15 h; soln. was filtered through Celite, volatiles were removed in vacuo; elem. anal.;
DOI:10.1021/om060115x