C₃₀H₃₉NO₄

Base Information

• Chemical Name: C₃₀H₃₉NO₄
• CAS No.: 1620849-86-6
• Molecular Formula: C₃₀H₃₉NO₄
• Molecular Weight: 477.644
• Mol file: 1620849-86-6.mol

Synonyms:C₃₀H₃₉NO₄

Chemical Property of C₃₀H₃₉NO₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₀H₃₉NO₄

There total 5 articles about C₃₀H₃₉NO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

C9H9ClO2 (1198577-72-8) + 2-((3S,8S,9S,10R,13S,14S,17S)-3-Hydroxy-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-17-yl)-propenal → C30H39NO4 (1620849-86-6)

Guidance literature:

C₉H₉ClO₂; With triethylamine;

2-((3S,8S,9S,10R,13S,14S,17S)-3-Hydroxy-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-17-yl)-propenal; In tetrahydrofuran; at 0 - 20 ℃; for 6h;

DOI:10.1016/j.steroids.2014.05.009

Reference yield:

prasterone acetate (853-23-6) → C30H39NO4 (1620849-86-6)

Guidance literature:

Multi-step reaction with 5 steps

1.1: ammonium acetate; acetic acid / toluene / Reflux

2.1: sodium tetrahydroborate / methanol

3.1: toluene-4-sulfonic acid / dichloromethane

4.1: diisobutylaluminium hydride / toluene / -78 °C

5.1: triethylamine

5.2: 6 h / 0 - 20 °C

With sodium tetrahydroborate; ammonium acetate; diisobutylaluminium hydride; toluene-4-sulfonic acid; acetic acid; triethylamine; In methanol; dichloromethane; toluene; 1.1: |Knoevenagel Condensation;

DOI:10.1016/j.steroids.2014.05.009

Reference yield:

3β-acetoxy-20ξ-cyano-5-pregnen-21-ol → C30H39NO4 (1620849-86-6)

Guidance literature:

Multi-step reaction with 3 steps

1.1: toluene-4-sulfonic acid / dichloromethane

2.1: diisobutylaluminium hydride / toluene / -78 °C

3.1: triethylamine

3.2: 6 h / 0 - 20 °C

With diisobutylaluminium hydride; toluene-4-sulfonic acid; triethylamine; In dichloromethane; toluene;

DOI:10.1016/j.steroids.2014.05.009

upstream raw materials:

C₉H₉ClO₂

prasterone acetate

ethyl 3β-acetoxy-20ξ-cyano-pregn-5,17(20)-dien-21-oate

C₂₉H₄₃NO₄