1-<2'-(β-N-Methylaminoethyl)-4',5'-dimethoxyphenyl>-2-(3'',4''-dimethoxyphenyl)-ethane

Base Information

Chemical Name:1-<2'-(β-N-Methylaminoethyl)-4',5'-dimethoxyphenyl>-2-(3'',4''-dimethoxyphenyl)-ethane
CAS No.:90601-59-5
Molecular Formula:C₂₁H₂₉NO₄
Molecular Weight:359.466
Hs Code.:

Synonyms:1-<2'-(β-N-Methylaminoethyl)-4',5'-dimethoxyphenyl>-2-(3'',4''-dimethoxyphenyl)-ethane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-<2'-(β-N-Methylaminoethyl)-4',5'-dimethoxyphenyl>-2-(3'',4''-dimethoxyphenyl)-ethane

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Technology Process of 1-<2'-(β-N-Methylaminoethyl)-4',5'-dimethoxyphenyl>-2-(3'',4''-dimethoxyphenyl)-ethane

There total 2 articles about 1-<2'-(β-N-Methylaminoethyl)-4',5'-dimethoxyphenyl>-2-(3'',4''-dimethoxyphenyl)-ethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 59643-48-0
2-(β-N-Benzyloxycarbonyl-N-methyl-aminoethyl)-4,5,3',4'-tetramethoxystilbene

: 90601-59-5
1-<2'-(β-N-Methylaminoethyl)-4',5'-dimethoxyphenyl>-2-(3'',4''-dimethoxyphenyl)-ethane

Guidance literature:: With hydrogen; palladium on activated charcoal; In chloroform; for 6h; Ambient temperature;
DOI:10.1002/ardp.19843170512

Reference yield:

: 1699-51-0,20412-65-1
laudanosine

: 90601-59-5
1-<2'-(β-N-Methylaminoethyl)-4',5'-dimethoxyphenyl>-2-(3'',4''-dimethoxyphenyl)-ethane

Guidance literature:: Multi-step reaction with 2 steps

1: 71 percent / 15percent aq. KOH / CHCl₃; diethyl ether / 2 h

2: 71 percent / H₂ / 10percent Pd/C / CHCl₃ / 6 h / Ambient temperature

With potassium hydroxide; hydrogen; palladium on activated charcoal; In diethyl ether; chloroform;
DOI:10.1002/ardp.19843170512