Ag(4-carbazol-9-yl-benzoic acid-H)

Base Information

• Chemical Name: Ag(4-carbazol-9-yl-benzoic acid-H)
• CAS No.: 937269-45-9
• Molecular Formula: Ag*C₁₉H₁₂NO₂
• Molecular Weight: 394.178
• Mol file: 937269-45-9.mol

Synonyms:Ag(4-carbazol-9-yl-benzoic acid-H)

Chemical Property of Ag(4-carbazol-9-yl-benzoic acid-H)

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of Ag(4-carbazol-9-yl-benzoic acid-H)

There total 1 articles about Ag(4-carbazol-9-yl-benzoic acid-H) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

4-(9H-carbazol-9-yl) benzoic acid (71935-21-2) + silver nitrate → Ag(4-carbazol-9-yl-benzoic acid-H) (937269-45-9)

Guidance literature:

With NaOH; In water; 4-carbazol-9-yl-benzoic acid (2 mmol) added to NaOH (2 mmol) soln.; stirred (30 min); filtered; soln. of AgNO3 (2 mmol) added (vigorous stirring); ppt. filtered; washed with H2O and ethanol; air-dried; elem. anal.;

DOI:10.1016/j.ica.2006.10.043

Reference yield: 82.0%

Ag(4-carbazol-9-yl-benzoic acid-H) (937269-45-9) + triphenylphosphine (603-35-0) → (triphenylphosphine)2Ag(4-carbazol-9-yl-benzoic acid-H) (937269-48-2)

Guidance literature:

In N,N-dimethyl-formamide; PPh3 (2 mmol) added to soln. of silver complex (1 mmol); heated (100°C, 10 min); filtered; kept (room temp., 10 h); elem. anal.;

DOI:10.1016/j.ica.2006.10.043

upstream raw materials:

4-(9H-carbazol-9-yl) benzoic acid

Downstream raw materials:

(triphenylphosphine)2Ag(4-carbazol-9-yl-benzoic acid-H)