2,7-dibromo-9,10-di[4-(O,O-diethylphosphonomethyl)phenyl]-phenanthrene

Base Information

• Chemical Name: 2,7-dibromo-9,10-di[4-(O,O-diethylphosphonomethyl)phenyl]-phenanthrene
• CAS No.: 1010812-20-0
• Molecular Formula: C₃₆H₃₈Br₂O₆P₂
• Molecular Weight: 788.45

Synonyms:2,7-dibromo-9,10-di[4-(O,O-diethylphosphonomethyl)phenyl]-phenanthrene

Chemical Property of 2,7-dibromo-9,10-di[4-(O,O-diethylphosphonomethyl)phenyl]-phenanthrene

Chemical Property:

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Technology Process of 2,7-dibromo-9,10-di[4-(O,O-diethylphosphonomethyl)phenyl]-phenanthrene

There total 1 articles about 2,7-dibromo-9,10-di[4-(O,O-diethylphosphonomethyl)phenyl]-phenanthrene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.7%

2,7-dibromo-9,10-di(4-bromomethylphenyl)-phenanthrene (1010812-19-7) + triethyl phosphite (122-52-1) → 2,7-dibromo-9,10-di[4-(O,O-diethylphosphonomethyl)phenyl]-phenanthrene (1010812-20-0)

Guidance literature:

for 7h; Reflux; Inert atmosphere;

DOI:10.1021/ol702873z

Reference yield: 90.4%

2,7-dibromo-9,10-di[4-(O,O-diethylphosphonomethyl)phenyl]-phenanthrene (1010812-20-0) + 3,4-bis(octyloxy)benzaldehyde (131525-50-3) → 2,7-dibromo-9,10-di[4-(3,4-bisoctyloxystyryl)-phenyl]-phenanthrene (1010812-21-1)

Guidance literature:

With potassium tert-butylate; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;

DOI:10.1021/ol702873z

upstream raw materials:

2,7-dibromo-9,10-di(4-bromomethylphenyl)-phenanthrene

triethyl phosphite

Downstream raw materials:

2,7-dibromo-9,10-di[4-(3,4-bisoctyloxystyryl)-phenyl]-phenanthrene

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