(2S,3S,E)-3-(1-(tert-butyldiphenylsilyl)pent-1-enyl)-N-phenyloxirane-2-carboxamide

Base Information

• Chemical Name: (2S,3S,E)-3-(1-(tert-butyldiphenylsilyl)pent-1-enyl)-N-phenyloxirane-2-carboxamide
• CAS No.: 949164-33-4
• Molecular Formula: C₃₀H₃₅NO₂Si
• Molecular Weight: 469.699

Synonyms:(2S,3S,E)-3-(1-(tert-butyldiphenylsilyl)pent-1-enyl)-N-phenyloxirane-2-carboxamide

Chemical Property of (2S,3S,E)-3-(1-(tert-butyldiphenylsilyl)pent-1-enyl)-N-phenyloxirane-2-carboxamide

Chemical Property:

Purity/Quality:

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Technology Process of (2S,3S,E)-3-(1-(tert-butyldiphenylsilyl)pent-1-enyl)-N-phenyloxirane-2-carboxamide

There total 1 articles about (2S,3S,E)-3-(1-(tert-butyldiphenylsilyl)pent-1-enyl)-N-phenyloxirane-2-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C22H28Si (949164-25-4) + 2-oxo-N-phenylacetamide (32331-75-2) → (2S,3S,E)-3-(1-(tert-butyldiphenylsilyl)pent-1-enyl)-N-phenyloxirane-2-carboxamide (949164-33-4) + (2R,3R,E)-3-(1-(tert-butyldiphenylsilyl)pent-1-enyl)-N-phenyloxirane-2-carboxamide

Guidance literature:

With 4 A molecular sieve; silver trifluoromethanesulfonate; In toluene; at -55 ℃; for 30h; Title compound not separated from byproducts.;

DOI:10.1021/ja0740420

Reference yield:

(2S,3S,E)-3-(1-(tert-butyldiphenylsilyl)pent-1-enyl)-N-phenyloxirane-2-carboxamide (949164-33-4) → [2S,(3,4,5S)]-2-hydroxy-N-phenylocta-3,4-dienamide

Guidance literature:

With sodium thiocyanide; In N,N-dimethyl-formamide; at 70 ℃;

DOI:10.1021/ja0740420

Reference yield:

(2S,3S,E)-3-(1-(tert-butyldiphenylsilyl)pent-1-enyl)-N-phenyloxirane-2-carboxamide (949164-33-4) → (2S,5R)-4-(tert-butyldiphenylsilyl)-N-phenyl-5-propyl-2,5-dihydrofuran-2-carboxamide

Guidance literature:

With iodine; In dichloromethane; at 0 - 20 ℃;

DOI:10.1021/ja0740420

upstream raw materials:

C₂₂H₂₈Si

2-oxo-N-phenylacetamide

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