2-hydroxyacetophenone-N-[(1R)-1-(methoxymethyl)propyl]-N-methylhydrazone

Base Information

Chemical Name:2-hydroxyacetophenone-N-[(1R)-1-(methoxymethyl)propyl]-N-methylhydrazone
CAS No.:281192-48-1
Molecular Formula:C₁₄H₂₂N₂O₂
Molecular Weight:250.341
Hs Code.:

Synonyms:2-hydroxyacetophenone-N-[(1R)-1-(methoxymethyl)propyl]-N-methylhydrazone

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Chemical Property of 2-hydroxyacetophenone-N-[(1R)-1-(methoxymethyl)propyl]-N-methylhydrazone

Chemical Property:

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Technology Process of 2-hydroxyacetophenone-N-[(1R)-1-(methoxymethyl)propyl]-N-methylhydrazone

There total 5 articles about 2-hydroxyacetophenone-N-[(1R)-1-(methoxymethyl)propyl]-N-methylhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.4%

: 118-93-4,104809-67-8
o-hydroxyacetophenone

: 281192-36-7
1-[(1R)-1-(methoxymethyl)propyl]-1-methylhydrazine

: 281192-48-1
2-hydroxyacetophenone-N-[(1R)-1-(methoxymethyl)propyl]-N-methylhydrazone

Guidance literature:: With toluene-4-sulfonic acid; In toluene; Heating;
DOI:10.1016/S0957-4166(00)00044-6

Reference yield:

: 57883-06-4
(R)-1-(methoxymethyl)propylamine

: 281192-48-1
2-hydroxyacetophenone-N-[(1R)-1-(methoxymethyl)propyl]-N-methylhydrazone

Guidance literature:: Multi-step reaction with 5 steps

1: 69.4 percent / 18 h / Heating

2: 52 percent / LiAlH₄ / diethyl ether / 8 h / Heating

3: 86.3 percent / sodium nitrite; aq. hydrochloric acid / 17 h / 20 °C

4: 99.5 percent / LiAlH₄ / diethyl ether / 20 °C

5: 94.4 percent / TsOH / toluene / Heating

With hydrogenchloride; lithium aluminium tetrahydride; toluene-4-sulfonic acid; sodium nitrite; In diethyl ether; toluene; 1: Formylation / 2: Reduction / 3: Nitrosation / 4: Reduction / 5: Condensation;
DOI:10.1016/S0957-4166(00)00044-6

Reference yield:

: 281192-34-5
(2R)-1-methoxy-N-methylbutan-2-amine

: 281192-48-1
2-hydroxyacetophenone-N-[(1R)-1-(methoxymethyl)propyl]-N-methylhydrazone

Guidance literature:: Multi-step reaction with 3 steps

1: 86.3 percent / sodium nitrite; aq. hydrochloric acid / 17 h / 20 °C

2: 99.5 percent / LiAlH₄ / diethyl ether / 20 °C

3: 94.4 percent / TsOH / toluene / Heating

With hydrogenchloride; lithium aluminium tetrahydride; toluene-4-sulfonic acid; sodium nitrite; In diethyl ether; toluene; 1: Nitrosation / 2: Reduction / 3: Condensation;
DOI:10.1016/S0957-4166(00)00044-6