methyl 14-cyclohexyl-5,6-dihydroxy-5,6,7,8-tetrahydroindolo[2,1-a][2]benzazocine-11-carboxylate

Base Information

• Chemical Name: methyl 14-cyclohexyl-5,6-dihydroxy-5,6,7,8-tetrahydroindolo[2,1-a][2]benzazocine-11-carboxylate
• CAS No.: 886042-43-9
• Molecular Formula: C₂₆H₂₉NO₄
• Molecular Weight: 419.521

Synonyms:methyl 14-cyclohexyl-5,6-dihydroxy-5,6,7,8-tetrahydroindolo[2,1-a][2]benzazocine-11-carboxylate

Chemical Property of methyl 14-cyclohexyl-5,6-dihydroxy-5,6,7,8-tetrahydroindolo[2,1-a][2]benzazocine-11-carboxylate

Chemical Property:

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Technology Process of methyl 14-cyclohexyl-5,6-dihydroxy-5,6,7,8-tetrahydroindolo[2,1-a][2]benzazocine-11-carboxylate

There total 1 articles about methyl 14-cyclohexyl-5,6-dihydroxy-5,6,7,8-tetrahydroindolo[2,1-a][2]benzazocine-11-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methyl 14-cyclohexyl-7,8-dihydroindolo[2,1-a][2]benzazocine-11-carboxylate (886042-41-7) → methyl 14-cyclohexyl-5,6-dihydroxy-5,6,7,8-tetrahydroindolo[2,1-a][2]benzazocine-11-carboxylate (886042-43-9)

Guidance literature:

With osmium(VIII) oxide; water; 4-methylmorpholine N-oxide; In tetrahydrofuran; acetone; at 20 ℃;

DOI:10.1055/s-0029-1217168

Reference yield:

methyl 14-cyclohexyl-5,6-dihydroxy-5,6,7,8-tetrahydroindolo[2,1-a][2]benzazocine-11-carboxylate (886042-43-9) + bis(trichloromethyl) carbonate (32315-10-9) → methyl 15-cyclohexyl-6-oxo-4b,7a,8,9-tetrahydro[1,3]dioxolo[4,5-e]indolo[2,1-a][2]benzazocine-12-carboxylate (886042-44-0)

Guidance literature:

With triethylamine; In dichloromethane; at -50 - 20 ℃; for 2.5h;

DOI:10.1055/s-0029-1217168

upstream raw materials:

methyl 14-cyclohexyl-7,8-dihydroindolo[2,1-a][2]benzazocine-11-carboxylate

Downstream raw materials:

methyl 15-cyclohexyl-6-oxo-4b,7a,8,9-tetrahydro[1,3]dioxolo[4,5-e]indolo[2,1-a][2]benzazocine-12-carboxylate

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