3-((R)-2-methylpiperidin-1-yl)-N-(4-((3-((S)-2-methylpiperidin-1-yl)propylamino)methyl)benzyl)propan-1-amine

Base Information

Chemical Name:3-((R)-2-methylpiperidin-1-yl)-N-(4-((3-((S)-2-methylpiperidin-1-yl)propylamino)methyl)benzyl)propan-1-amine
CAS No.:1394847-39-2
Molecular Formula:C₂₆H₄₆N₄
Molecular Weight:414.678
Hs Code.:

Synonyms:3-((R)-2-methylpiperidin-1-yl)-N-(4-((3-((S)-2-methylpiperidin-1-yl)propylamino)methyl)benzyl)propan-1-amine

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Chemical Property of 3-((R)-2-methylpiperidin-1-yl)-N-(4-((3-((S)-2-methylpiperidin-1-yl)propylamino)methyl)benzyl)propan-1-amine

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Technology Process of 3-((R)-2-methylpiperidin-1-yl)-N-(4-((3-((S)-2-methylpiperidin-1-yl)propylamino)methyl)benzyl)propan-1-amine

There total 12 articles about 3-((R)-2-methylpiperidin-1-yl)-N-(4-((3-((S)-2-methylpiperidin-1-yl)propylamino)methyl)benzyl)propan-1-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3-((R)-2-methylpiperidin-1-yl)-N-(4-((3-((S)-2-methylpiperidin-1-yl)propylamino)methyl)benzyl)propan-1-amine

: 1394847-39-2
3-((R)-2-methylpiperidin-1-yl)-N-(4-((3-((S)-2-methylpiperidin-1-yl)propylamino)methyl)benzyl)propan-1-amine

Guidance literature:: With sodium tetrahydroborate; In methanol; at 0 - 20 ℃;
DOI:10.1021/jm300862u

Reference yield:

: 5119-88-0,205526-61-0
(+)-(2R)-2-methylpiperidine hydrochloride

: 1394847-39-2
3-((R)-2-methylpiperidin-1-yl)-N-(4-((3-((S)-2-methylpiperidin-1-yl)propylamino)methyl)benzyl)propan-1-amine

Guidance literature:: Multi-step reaction with 5 steps

1: sodium hydroxide / water

2: potassium carbonate / acetonitrile / 8 h / Reflux

3: hydrazine hydrate / ethanol / 1 h / Reflux

4: sodium sulfate / methanol / 24 h / Reflux; Inert atmosphere

5: sodium tetrahydroborate / methanol / 0 - 20 °C

With sodium tetrahydroborate; potassium carbonate; hydrazine hydrate; sodium sulfate; sodium hydroxide; In methanol; ethanol; water; acetonitrile;
DOI:10.1021/jm300862u

Reference yield:

: 1394847-65-4
(S)-4-((3-(2-methylpiperidin-1-yl)propylamino)methyl)benzaldehyde

: 1394847-39-2
3-((R)-2-methylpiperidin-1-yl)-N-(4-((3-((S)-2-methylpiperidin-1-yl)propylamino)methyl)benzyl)propan-1-amine

Guidance literature:: Multi-step reaction with 2 steps

1: sodium sulfate / methanol / 24 h / Reflux; Inert atmosphere

2: sodium tetrahydroborate / methanol / 0 - 20 °C

With sodium tetrahydroborate; sodium sulfate; In methanol;
DOI:10.1021/jm300862u