(S)-3-(1H-indol-2-yl)-1-oxo-1-(phenylthio)propan-2-aminium chloride

Base Information

Chemical Name:(S)-3-(1H-indol-2-yl)-1-oxo-1-(phenylthio)propan-2-aminium chloride
CAS No.:1147996-30-2
Molecular Formula:C₁₇H₁₆N₂OS*ClH
Molecular Weight:332.854
Hs Code.:

Synonyms:(S)-3-(1H-indol-2-yl)-1-oxo-1-(phenylthio)propan-2-aminium chloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-3-(1H-indol-2-yl)-1-oxo-1-(phenylthio)propan-2-aminium chloride

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Technology Process of (S)-3-(1H-indol-2-yl)-1-oxo-1-(phenylthio)propan-2-aminium chloride

There total 3 articles about (S)-3-(1H-indol-2-yl)-1-oxo-1-(phenylthio)propan-2-aminium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1360878-92-7
C₂₂H₂₄N₂O₃S

: 1147996-30-2
(S)-3-(1H-indol-2-yl)-1-oxo-1-(phenylthio)propan-2-aminium chloride

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1002/anie.201107482

Reference yield:

: 13139-14-5
Boc-Trp-OH

: 1147996-30-2
(S)-3-(1H-indol-2-yl)-1-oxo-1-(phenylthio)propan-2-aminium chloride

Guidance literature:: Multi-step reaction with 2 steps

1: dicyclohexyl-carbodiimide / ethyl acetate / 1.5 h / 0 - 20 °C / Inert atmosphere

2: hydrogenchloride / 1,4-dioxane / 1 h / 20 °C / Inert atmosphere

With hydrogenchloride; dicyclohexyl-carbodiimide; In 1,4-dioxane; ethyl acetate;
DOI:10.1002/anie.201107482

Reference yield:

: 108-98-5
thiophenol

: 1147996-30-2
(S)-3-(1H-indol-2-yl)-1-oxo-1-(phenylthio)propan-2-aminium chloride

Guidance literature:: Multi-step reaction with 2 steps

1: dicyclohexyl-carbodiimide / ethyl acetate / 1.5 h / 0 - 20 °C / Inert atmosphere

2: hydrogenchloride / 1,4-dioxane / 1 h / 20 °C / Inert atmosphere

With hydrogenchloride; dicyclohexyl-carbodiimide; In 1,4-dioxane; ethyl acetate;
DOI:10.1002/anie.201107482