methyl 3-(N-benzoyl)amino-4,4,4-trifluoro-3-trifluoromethyl-2-methylenebutanoate

Base Information

• Chemical Name: methyl 3-(N-benzoyl)amino-4,4,4-trifluoro-3-trifluoromethyl-2-methylenebutanoate
• CAS No.: 336625-00-4
• Molecular Formula: C₁₄H₁₁F₆NO₃
• Molecular Weight: 355.237

Synonyms:methyl 3-(N-benzoyl)amino-4,4,4-trifluoro-3-trifluoromethyl-2-methylenebutanoate

Chemical Property of methyl 3-(N-benzoyl)amino-4,4,4-trifluoro-3-trifluoromethyl-2-methylenebutanoate

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Technology Process of methyl 3-(N-benzoyl)amino-4,4,4-trifluoro-3-trifluoromethyl-2-methylenebutanoate

There total 2 articles about methyl 3-(N-benzoyl)amino-4,4,4-trifluoro-3-trifluoromethyl-2-methylenebutanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

N-(2,2,2-trifluoro-1-trifluoromethyl-ethylidene)-benzamide (5022-41-3) + acrylic acid methyl ester (292638-85-8,9003-21-8,96-33-3) → methyl 3-(N-benzoyl)amino-4,4,4-trifluoro-3-trifluoromethyl-2-methylenebutanoate (336625-00-4)

Guidance literature:

With 1,4-diaza-bicyclo[2.2.2]octane; calcium hydride; In tetrahydrofuran; at 20 ℃; for 48h;

DOI:10.1055/s-2001-10816

Reference yield:

N-(2,2,2-trifluoro-1-trifluoromethyl-ethylidene)-benzamide (5022-41-3) + [α-(methoxycarbonyl)vinyl]diisobutylaluminum (107270-46-2) → methyl 3-(N-benzoyl)amino-4,4,4-trifluoro-3-trifluoromethyl-2-methylenebutanoate (336625-00-4)

Guidance literature:

With boron trifluoride diethyl etherate; In tetrahydrofuran; at 20 ℃;

DOI:10.1016/S0022-1139(01)00434-1

Reference yield: 90.0%

methyl 3-(N-benzoyl)amino-4,4,4-trifluoro-3-trifluoromethyl-2-methylenebutanoate (336625-00-4) → Methyl 3-(N-benzoyl)amino-4,4,4-trifluoro-3-trifluoromethyl-2-methylbutanoate (336625-04-8)

Guidance literature:

With hydrogen; palladium on activated charcoal; In methanol; for 72h;

DOI:10.1055/s-2001-10816

upstream raw materials:

N-(2,2,2-trifluoro-1-trifluoromethyl-ethylidene)-benzamide

acrylic acid methyl ester

[α-(methoxycarbonyl)vinyl]diisobutylaluminum

Downstream raw materials:

Methyl 3-(N-benzoyl)amino-4,4,4-trifluoro-3-trifluoromethyl-2-methylbutanoate

2-Phenyl-4,4-bis(trifluoromethyl)-5-methyl-1,3-oxazin-6-one

3-(N-Benzoyl)amino-4,4,4-trifluoro-3-trifluoromethyl-2-methylbutanoic acid

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