4-(diethoxyphosphorylmethyl)-1,2-diaminophenyl

Base Information

Chemical Name:4-(diethoxyphosphorylmethyl)-1,2-diaminophenyl
CAS No.:773057-68-4
Molecular Formula:C₁₁H₁₉N₂O₃P
Molecular Weight:258.257
Hs Code.:

Synonyms:4-(diethoxyphosphorylmethyl)-1,2-diaminophenyl

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-(diethoxyphosphorylmethyl)-1,2-diaminophenyl

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Technology Process of 4-(diethoxyphosphorylmethyl)-1,2-diaminophenyl

There total 3 articles about 4-(diethoxyphosphorylmethyl)-1,2-diaminophenyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 791856-15-0
4-(diethoxyphosphorylmethyl)-1-phthalamido-2-nitro-phenyl

: 773057-68-4
4-(diethoxyphosphorylmethyl)-1,2-diaminophenyl

Guidance literature:: With hydrazine hydrate; palladium on activated charcoal; In ethanol; for 3h; Heating;
DOI:10.1016/j.tetlet.2004.07.067

Reference yield:

: 20074-79-7
diethyl (4-aminobenzyl)phosphonate

: 773057-68-4
4-(diethoxyphosphorylmethyl)-1,2-diaminophenyl

Guidance literature:: Multi-step reaction with 3 steps

1: 91 percent / acetic acid / 3 h / Heating

2: 87 percent / HNO₃; H₂SO₄ / -5 - 20 °C

3: 65 percent / hydrazine monohydrate / Pd/C / ethanol / 3 h / Heating

With sulfuric acid; nitric acid; hydrazine hydrate; palladium on activated charcoal; In ethanol; acetic acid;
DOI:10.1016/j.tetlet.2004.07.067

Reference yield:

: 4-(diethoxyphosphorylmethyl)-1-phthalamido-phenyl

: 773057-68-4
4-(diethoxyphosphorylmethyl)-1,2-diaminophenyl

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / HNO₃; H₂SO₄ / -5 - 20 °C

2: 65 percent / hydrazine monohydrate / Pd/C / ethanol / 3 h / Heating

With sulfuric acid; nitric acid; hydrazine hydrate; palladium on activated charcoal; In ethanol;
DOI:10.1016/j.tetlet.2004.07.067