tert-butyl pent-3-ynyl(phenyl)carbamate

Base Information

Chemical Name:tert-butyl pent-3-ynyl(phenyl)carbamate
CAS No.:1189536-80-8
Molecular Formula:C₁₆H₂₁NO₂
Molecular Weight:259.348
Hs Code.:

Synonyms:tert-butyl pent-3-ynyl(phenyl)carbamate

Suppliers and Price of tert-butyl pent-3-ynyl(phenyl)carbamate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of tert-butyl pent-3-ynyl(phenyl)carbamate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of tert-butyl pent-3-ynyl(phenyl)carbamate

There total 1 articles about tert-butyl pent-3-ynyl(phenyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 106060-18-8
methanesulfonic acid pent-3-ynyl ester

: 62-53-3
aniline

: 1189536-80-8
tert-butyl pent-3-ynyl(phenyl)carbamate

: 1189537-29-8
N,N-di(pent-3-ynyl)aniline

Guidance literature:: methanesulfonic acid pent-3-ynyl ester; aniline; With potassium carbonate; In acetonitrile; at 0 ℃; Inert atmosphere; Reflux;

di-tert-butyl dicarbonate; at 130 ℃; for 0.75h; Inert atmosphere;
DOI:10.1016/j.tet.2009.07.015

Reference yield: 41.0%

: 1189536-80-8
tert-butyl pent-3-ynyl(phenyl)carbamate

: 1189537-19-6
(E)-3-ethylidene-1-phenylpyrrolidin-2-one

: 1189537-32-3
(Z)-tert-butyl pent-3-enyl(phenyl)carbamate

Guidance literature:: tert-butyl pent-3-ynyl(phenyl)carbamate; With titanium(IV) isopropylate; cyclopentylmagnesium chloride; In diethyl ether; at -70 - 0 ℃; Inert atmosphere;

With hydrogenchloride; water; In diethyl ether; at 0 ℃; diastereoselective reaction; Inert atmosphere;
DOI:10.1016/j.tet.2009.07.015

Reference yield: 26.0%

: 1189536-80-8
tert-butyl pent-3-ynyl(phenyl)carbamate

: 105-58-8,76619-83-5
Diethyl carbonate

: 1189537-19-6
(E)-3-ethylidene-1-phenylpyrrolidin-2-one

: 1189536-95-5
(E)-ethyl 5-(tert-butoxycarbonyl(phenyl)amino)-2-methylpent-2-enoate

: 1189536-96-6
(E)-ethyl 2-(2-(tert-butoxycarbonyl(phenyl)amino)ethyl)-but-2-enoate

Guidance literature:: tert-butyl pent-3-ynyl(phenyl)carbamate; Diethyl carbonate; With titanium(IV) isopropylate; cyclopentylmagnesium chloride; In diethyl ether; at 0 ℃; Inert atmosphere;

With hydrogenchloride; water; In diethyl ether; at 0 ℃; diastereoselective reaction; Inert atmosphere;
DOI:10.1016/j.tet.2009.07.015