(-)-[(1S,2R,4R)-(2-hydroxy-7,7-dimethylbicyclo[2.2.1]-1-yl)methylsulfanyl]-N-[2-(3,4-dimethoxyphenyl)ethyl]succinimide

Base Information

Chemical Name:(-)-[(1S,2R,4R)-(2-hydroxy-7,7-dimethylbicyclo[2.2.1]-1-yl)methylsulfanyl]-N-[2-(3,4-dimethoxyphenyl)ethyl]succinimide
CAS No.:446063-57-6
Molecular Formula:C₂₄H₃₃NO₅S
Molecular Weight:447.596
Hs Code.:

Synonyms:(-)-[(1S,2R,4R)-(2-hydroxy-7,7-dimethylbicyclo[2.2.1]-1-yl)methylsulfanyl]-N-[2-(3,4-dimethoxyphenyl)ethyl]succinimide

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Chemical Property of (-)-[(1S,2R,4R)-(2-hydroxy-7,7-dimethylbicyclo[2.2.1]-1-yl)methylsulfanyl]-N-[2-(3,4-dimethoxyphenyl)ethyl]succinimide

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Technology Process of (-)-[(1S,2R,4R)-(2-hydroxy-7,7-dimethylbicyclo[2.2.1]-1-yl)methylsulfanyl]-N-[2-(3,4-dimethoxyphenyl)ethyl]succinimide

There total 1 articles about (-)-[(1S,2R,4R)-(2-hydroxy-7,7-dimethylbicyclo[2.2.1]-1-yl)methylsulfanyl]-N-[2-(3,4-dimethoxyphenyl)ethyl]succinimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 37597-19-6
1‐(3,4‐dimethoxyphenethyl)‐1H‐pyrrole‐2,5‐dione

: 71242-58-5
(1S,2R,4R)-(-)-10-mercaptoisoboneol

: 446063-57-6
(-)-[(1S,2R,4R)-(2-hydroxy-7,7-dimethylbicyclo[2.2.1]-1-yl)methylsulfanyl]-N-[2-(3,4-dimethoxyphenyl)ethyl]succinimide

Guidance literature:: With triethylamine; at 0 - 20 ℃; for 24h;
DOI:10.1055/s-2002-22703

Reference yield: 84.0%

: 446063-57-6
(-)-[(1S,2R,4R)-(2-hydroxy-7,7-dimethylbicyclo[2.2.1]-1-yl)methylsulfanyl]-N-[2-(3,4-dimethoxyphenyl)ethyl]succinimide

: 446063-58-7
(-)-[(1S,2R,4R)-(2-hydroxy-7,7-dimethylbicyclo[2.2.1]-1-yl)methylsulfanyl]-N-[2-(3,4-dimethoxyphenyl)ethyl]maleimide

Guidance literature:: With N-chloro-succinimide; In tetrachloromethane; for 16h; Heating;
DOI:10.1055/s-2002-22703 DOI:10.1021/jo049672o

Reference yield:

: 446063-57-6
(-)-[(1S,2R,4R)-(2-hydroxy-7,7-dimethylbicyclo[2.2.1]-1-yl)methylsulfanyl]-N-[2-(3,4-dimethoxyphenyl)ethyl]succinimide

: 446063-56-5
(2R,6S)-4-[2-(3,4-dimethoxyphenyl)ethyl]-2-[(1S,2R,4R,S_R)-(2-hydroxy-7,7-dimethylbicyclo[2.2.1]hept-1-yl)methylsulfinyl]-4-aza-tricyclo[5.2.1.0^2,6]dec-8-ene-3,5-dione

Guidance literature:: Multi-step reaction with 3 steps

1: 84 percent / NCS / CCl₄ / 16 h / Heating

2: 97 percent / MCPBA / CH₂Cl₂ / 0 - 20 °C

3: CH₂Cl₂ / 0 °C

With N-chloro-succinimide; 3-chloro-benzenecarboperoxoic acid; In tetrachloromethane; dichloromethane; 3: Diels-Alder reaction;
DOI:10.1021/jo049672o