5,11,17,23-tetrakis(1,1-dimethylethyl)-25,26,27,28-N-benzilideneamino-2,8,14,20-tetrathiapentacyclo[19.3.1.1(3,7).1(9,13).1(15,19)]octacosa-1⁽²⁵⁾,3,5,7⁽²⁸⁾,9,11,13⁽²⁷⁾,15,17,19⁽²⁶⁾,21,23-dodecaene-2,8,14,20-tetraoxide

Base Information

• Chemical Name: 5,11,17,23-tetrakis(1,1-dimethylethyl)-25,26,27,28-N-benzilideneamino-2,8,14,20-tetrathiapentacyclo[19.3.1.1(3,7).1(9,13).1(15,19)]octacosa-1⁽²⁵⁾,3,5,7⁽²⁸⁾,9,11,13⁽²⁷⁾,15,17,19⁽²⁶⁾,21,23-dodecaene-2,8,14,20-tetraoxide
• CAS No.: 329325-96-4
• Molecular Formula: C₆₈H₆₈N₄O₄S₄
• Molecular Weight: 1133.58

Synonyms:5,11,17,23-tetrakis(1,1-dimethylethyl)-25,26,27,28-N-benzilideneamino-2,8,14,20-tetrathiapentacyclo[19.3.1.1(3,7).1(9,13).1(15,19)]octacosa-1⁽²⁵⁾,3,5,7⁽²⁸⁾,9,11,13⁽²⁷⁾,15,17,19⁽²⁶⁾,21,23-dodecaene-2,8,14,20-tetraoxide

Chemical Property of 5,11,17,23-tetrakis(1,1-dimethylethyl)-25,26,27,28-N-benzilideneamino-2,8,14,20-tetrathiapentacyclo[19.3.1.1(3,7).1(9,13).1(15,19)]octacosa-1⁽²⁵⁾,3,5,7⁽²⁸⁾,9,11,13⁽²⁷⁾,15,17,19⁽²⁶⁾,21,23-dodecaene-2,8,14,20-tetraoxide

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Technology Process of 5,11,17,23-tetrakis(1,1-dimethylethyl)-25,26,27,28-N-benzilideneamino-2,8,14,20-tetrathiapentacyclo[19.3.1.1(3,7).1(9,13).1(15,19)]octacosa-1⁽²⁵⁾,3,5,7⁽²⁸⁾,9,11,13⁽²⁷⁾,15,17,19⁽²⁶⁾,21,23-dodecaene-2,8,14,20-tetraoxide

There total 3 articles about 5,11,17,23-tetrakis(1,1-dimethylethyl)-25,26,27,28-N-benzilideneamino-2,8,14,20-tetrathiapentacyclo[19.3.1.1(3,7).1(9,13).1(15,19)]octacosa-1⁽²⁵⁾,3,5,7⁽²⁸⁾,9,11,13⁽²⁷⁾,15,17,19⁽²⁶⁾,21,23-dodecaene-2,8,14,20-tetraoxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

5,11,17,23-tetrakis(1,1-dimethylethyl)-25,26,27,28-tetrakis(N-benzylamino)-2,8,14,20-tetrathiapentacyclo[19.3.1.1(3,7).1(9,13).1(15,19)]octacosa-1(25),3,5,7(28),9,11,13(27),15,17,19(26),21,23-dodecaene-2,8,14,20-tetraoxide (329325-95-3) → 5,11,17,23-tetrakis(1,1-dimethylethyl)-25,26,27,28-N-benzilideneamino-2,8,14,20-tetrathiapentacyclo[19.3.1.1(3,7).1(9,13).1(15,19)]octacosa-1(25),3,5,7(28),9,11,13(27),15,17,19(26),21,23-dodecaene-2,8,14,20-tetraoxide (329325-96-4)

Guidance literature:

With N-Bromosuccinimide; dibenzoyl peroxide; In benzene; for 1h; Heating;

DOI:10.1021/ja005573q

Reference yield:

benzylamine (100-46-9) → 5,11,17,23-tetrakis(1,1-dimethylethyl)-25,26,27,28-N-benzilideneamino-2,8,14,20-tetrathiapentacyclo[19.3.1.1(3,7).1(9,13).1(15,19)]octacosa-1(25),3,5,7(28),9,11,13(27),15,17,19(26),21,23-dodecaene-2,8,14,20-tetraoxide (329325-96-4)

Guidance literature:

Multi-step reaction with 2 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / 0 °C

1.2: 64 percent / tetrahydrofuran; hexane / 2 h / 20 °C

2.1: 85 percent / N-bromosuccinimide; dibenzoyl peroxide / benzene / 1 h / Heating

With N-Bromosuccinimide; n-butyllithium; dibenzoyl peroxide; In tetrahydrofuran; hexane; benzene;

DOI:10.1021/ja005573q

Reference yield:

5,11,17,23-tetrakis(1,1-dimethylethyl)-25,26,27,28-tetramethoxy-2,8,14,20-tetrathiapentacyclo[19.3.1.1(3,7).1(9,13).1(15,19)]octacosa-1(25),3,5,7(28),9,11,13(27),15,17,19(26),21,23-dodecaene-2,8,14,20-tetraoxide (204190-45-4,518034-43-0,518034-44-1,518034-45-2,518034-46-3) → 5,11,17,23-tetrakis(1,1-dimethylethyl)-25,26,27,28-N-benzilideneamino-2,8,14,20-tetrathiapentacyclo[19.3.1.1(3,7).1(9,13).1(15,19)]octacosa-1(25),3,5,7(28),9,11,13(27),15,17,19(26),21,23-dodecaene-2,8,14,20-tetraoxide (329325-96-4)

Guidance literature:

Multi-step reaction with 2 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / 0 °C

1.2: 64 percent / tetrahydrofuran; hexane / 2 h / 20 °C

2.1: 85 percent / N-bromosuccinimide; dibenzoyl peroxide / benzene / 1 h / Heating

With N-Bromosuccinimide; n-butyllithium; dibenzoyl peroxide; In tetrahydrofuran; hexane; benzene;

DOI:10.1021/ja005573q

upstream raw materials:

5,11,17,23-tetrakis(1,1-dimethylethyl)-25,26,27,28-tetrakis(N-benzylamino)-2,8,14,20-tetrathiapentacyclo[19.3.1.1(3,7).1(9,13).1(15,19)]octacosa-1⁽²⁵⁾,3,5,7⁽²⁸⁾,9,11,13⁽²⁷⁾,15,17,19⁽²⁶⁾,21,23-dodecaene-2,8,14,20-tetraoxide

benzylamine

5,11,17,23-tetrakis(1,1-dimethylethyl)-25,26,27,28-tetramethoxy-2,8,14,20-tetrathiapentacyclo[19.3.1.1(3,7).1(9,13).1(15,19)]octacosa-1⁽²⁵⁾,3,5,7⁽²⁸⁾,9,11,13⁽²⁷⁾,15,17,19⁽²⁶⁾,21,23-dodecaene-2,8,14,20-tetraoxide

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