Technology Process of C32H30Cl4N2O3
There total 7 articles about C32H30Cl4N2O3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
zinc(II) chloride;
at 250 ℃;
for 0.0333333h;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: sodium acetate / water; ethanol / 16 h / Reflux
2.1: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / Reflux
3.1: potassium carbonate / acetonitrile / 18 h / Reflux
4.1: boron tribromide / dichloromethane / 3 h / -78 - -20 °C
4.2: -20 - 20 °C
5.1: zinc(II) chloride / 0.03 h / 250 °C
With
lithium aluminium tetrahydride; sodium acetate; boron tribromide; potassium carbonate; zinc(II) chloride;
In
tetrahydrofuran; ethanol; dichloromethane; water; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: potassium carbonate / acetonitrile / 18 h / Reflux
2.1: boron tribromide / dichloromethane / 3 h / -78 - -20 °C
2.2: -20 - 20 °C
3.1: zinc(II) chloride / 0.03 h / 250 °C
With
boron tribromide; potassium carbonate; zinc(II) chloride;
In
dichloromethane; acetonitrile;