N^α-(tert-butyldimethylsilyloxycarbonyl)-N^ε-(benzyloxycarbonyl)-L-lysine methyl ester

Base Information

• Chemical Name: N^α-(tert-butyldimethylsilyloxycarbonyl)-N^ε-(benzyloxycarbonyl)-L-lysine methyl ester
• CAS No.: 108634-98-6
• Molecular Formula: C₂₂H₃₆N₂O₆Si
• Molecular Weight: 452.623

Synonyms:N^α-(tert-butyldimethylsilyloxycarbonyl)-N^ε-(benzyloxycarbonyl)-L-lysine methyl ester

Chemical Property of N^α-(tert-butyldimethylsilyloxycarbonyl)-N^ε-(benzyloxycarbonyl)-L-lysine methyl ester

Chemical Property:

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Technology Process of N^α-(tert-butyldimethylsilyloxycarbonyl)-N^ε-(benzyloxycarbonyl)-L-lysine methyl ester

There total 1 articles about N^α-(tert-butyldimethylsilyloxycarbonyl)-N^ε-(benzyloxycarbonyl)-L-lysine methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

t-butyldimethylsiyl triflate (69739-34-0) + Boc-L-Lys(Z)-OMe (73548-77-3) → Nα-(tert-butyldimethylsilyloxycarbonyl)-Nε-(benzyloxycarbonyl)-L-lysine methyl ester (108634-98-6)

Guidance literature:

With 2,6-dimethylpyridine; In dichloromethane; Ambient temperature;

DOI:10.1016/S0040-4039(00)83871-X

Reference yield:

Nα-(tert-butyldimethylsilyloxycarbonyl)-Nε-(benzyloxycarbonyl)-L-lysine methyl ester (108634-98-6) → (S)-methyl 2-amino-6-(benzyloxycarbonylamino)hexanoate (24498-31-5)

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran; for 1h; Yield given; Ambient temperature;

DOI:10.1021/jo00290a015

upstream raw materials:

t-butyldimethylsiyl triflate

Boc-L-Lys(Z)-OMe

Downstream raw materials:

(S)-methyl 2-amino-6-(benzyloxycarbonylamino)hexanoate

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