C₄₅H₇₁N₇O₉

Base Information

Chemical Name:C₄₅H₇₁N₇O₉
CAS No.:252353-77-8
Molecular Formula:C₄₅H₇₁N₇O₉
Molecular Weight:854.1
Hs Code.:

C<sub>45</sub>H<sub>71</sub>N<sub>7</sub>O<sub>9</sub>

Synonyms:C₄₅H₇₁N₇O₉

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Chemical Property of C₄₅H₇₁N₇O₉

Chemical Property:

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Technology Process of C₄₅H₇₁N₇O₉

There total 13 articles about C₄₅H₇₁N₇O₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 768-03-6,26742-84-7
Phenyl vinyl ketone

: 252353-77-8
C₄₅H₇₁N₇O₉

Guidance literature:: Multi-step reaction with 12 steps

1: methanol / 2 h / 40 °C

2: NaBH₄ / ethanol / 3 h / 10 °C

3: H₂ / 10 percent Pd/C / methanol / 6 h / 20 °C / 760 Torr

4: KI; Na₂CO₃ / butan-1-ol / 2 h / Heating

5: Et₃N / CH₂Cl₂ / 1 h

6: NaN₃ / dimethylsulfoxide / 15 h / 40 - 45 °C

7: H₂ / 10 percent Pd/C / ethyl acetate / 15 h / 20 °C / 3000.24 Torr

8: H₂; NH₃ / Raney Ni / ethanol / 15 h / 20 °C / 4500.36 Torr

9: Et₃N / toluene / 15 h / 80 °C

10: 1N NaOH / 1,2-dimethoxy-ethane / 15 h / 20 °C

11: N-methylmorpholine / tetrahydrofuran / 0.5 h / -30 °C

12: tetrahydrofuran / 2 h / 20 °C

With 4-methyl-morpholine; sodium hydroxide; sodium tetrahydroborate; sodium azide; ammonia; hydrogen; sodium carbonate; triethylamine; potassium iodide; palladium on activated charcoal; nickel; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; ethanol; dichloromethane; dimethyl sulfoxide; ethyl acetate; toluene; butan-1-ol; 1: Addition / 2: Reduction / 3: Hydrogenolysis / 4: Alkylation / 5: Mesylation / 6: Substitution / 7: Reduction-tert-butyloxycarbonylation / 8: Catalytic hydrogenation / 9: Condensation / 10: Hydrolysis / 11: Acylation / 12: Condensation;
DOI:10.1021/jm991043x

Reference yield:

: 122377-71-3
3-(N,N-Dibenzylamino)-1-phenyl-propan-1-on

: 252353-77-8
C₄₅H₇₁N₇O₉

Guidance literature:: Multi-step reaction with 11 steps

1: NaBH₄ / ethanol / 3 h / 10 °C

2: H₂ / 10 percent Pd/C / methanol / 6 h / 20 °C / 760 Torr

3: KI; Na₂CO₃ / butan-1-ol / 2 h / Heating

4: Et₃N / CH₂Cl₂ / 1 h

5: NaN₃ / dimethylsulfoxide / 15 h / 40 - 45 °C

6: H₂ / 10 percent Pd/C / ethyl acetate / 15 h / 20 °C / 3000.24 Torr

7: H₂; NH₃ / Raney Ni / ethanol / 15 h / 20 °C / 4500.36 Torr

8: Et₃N / toluene / 15 h / 80 °C

9: 1N NaOH / 1,2-dimethoxy-ethane / 15 h / 20 °C

10: N-methylmorpholine / tetrahydrofuran / 0.5 h / -30 °C

11: tetrahydrofuran / 2 h / 20 °C

With 4-methyl-morpholine; sodium hydroxide; sodium tetrahydroborate; sodium azide; ammonia; hydrogen; sodium carbonate; triethylamine; potassium iodide; palladium on activated charcoal; nickel; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; ethanol; dichloromethane; dimethyl sulfoxide; ethyl acetate; toluene; butan-1-ol; 1: Reduction / 2: Hydrogenolysis / 3: Alkylation / 4: Mesylation / 5: Substitution / 6: Reduction-tert-butyloxycarbonylation / 7: Catalytic hydrogenation / 8: Condensation / 9: Hydrolysis / 10: Acylation / 11: Condensation;
DOI:10.1021/jm991043x

Reference yield:

: 34597-73-4
3-(Benzylamino)-1-phenyl-1-propanol

: 252353-77-8
C₄₅H₇₁N₇O₉

Guidance literature:: Multi-step reaction with 9 steps

1: KI; Na₂CO₃ / butan-1-ol / 2 h / Heating

2: Et₃N / CH₂Cl₂ / 1 h

3: NaN₃ / dimethylsulfoxide / 15 h / 40 - 45 °C

4: H₂ / 10 percent Pd/C / ethyl acetate / 15 h / 20 °C / 3000.24 Torr

5: H₂; NH₃ / Raney Ni / ethanol / 15 h / 20 °C / 4500.36 Torr

6: Et₃N / toluene / 15 h / 80 °C

7: 1N NaOH / 1,2-dimethoxy-ethane / 15 h / 20 °C

8: N-methylmorpholine / tetrahydrofuran / 0.5 h / -30 °C

9: tetrahydrofuran / 2 h / 20 °C

With 4-methyl-morpholine; sodium hydroxide; sodium azide; ammonia; hydrogen; sodium carbonate; triethylamine; potassium iodide; palladium on activated charcoal; nickel; In tetrahydrofuran; 1,2-dimethoxyethane; ethanol; dichloromethane; dimethyl sulfoxide; ethyl acetate; toluene; butan-1-ol; 1: Alkylation / 2: Mesylation / 3: Substitution / 4: Reduction-tert-butyloxycarbonylation / 5: Catalytic hydrogenation / 6: Condensation / 7: Hydrolysis / 8: Acylation / 9: Condensation;
DOI:10.1021/jm991043x