2-acetamido-2-(2-{4-[3-(benzyloxy)phenylthio]-2-chlorophenyl}ethyl)malonic acid diethyl ester

Base Information

• Chemical Name: 2-acetamido-2-(2-{4-[3-(benzyloxy)phenylthio]-2-chlorophenyl}ethyl)malonic acid diethyl ester
• CAS No.: 1023648-21-6
• Molecular Formula: C₃₀H₃₂ClNO₆S
• Molecular Weight: 570.106

Synonyms:2-acetamido-2-(2-{4-[3-(benzyloxy)phenylthio]-2-chlorophenyl}ethyl)malonic acid diethyl ester

Chemical Property of 2-acetamido-2-(2-{4-[3-(benzyloxy)phenylthio]-2-chlorophenyl}ethyl)malonic acid diethyl ester

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Technology Process of 2-acetamido-2-(2-{4-[3-(benzyloxy)phenylthio]-2-chlorophenyl}ethyl)malonic acid diethyl ester

There total 1 articles about 2-acetamido-2-(2-{4-[3-(benzyloxy)phenylthio]-2-chlorophenyl}ethyl)malonic acid diethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

3-[3-(benzyloxy)phenylthio]-6-vinyl-1-chlorobenzene (1023648-20-5) + 2-acetylaminomalonic acid diethyl ester (1068-90-2) → 2-acetamido-2-(2-{4-[3-(benzyloxy)phenylthio]-2-chlorophenyl}ethyl)malonic acid diethyl ester (1023648-21-6) + triethyl 2-(acetylamino)ethylene-1,1,2-tricarboxylate

Guidance literature:

2-acetylaminomalonic acid diethyl ester; With caesium carbonate; In dimethyl sulfoxide; at 20 ℃; for 0.5h;

3-[3-(benzyloxy)phenylthio]-6-vinyl-1-chlorobenzene; In dimethyl sulfoxide; at 20 - 35 ℃; Further stages.;

DOI:10.1016/j.tet.2008.01.086

Reference yield: 95.0%

2-acetamido-2-(2-{4-[3-(benzyloxy)phenylthio]-2-chlorophenyl}ethyl)malonic acid diethyl ester (1023648-21-6) → N-(3-{4-[3-(benzyloxy)phenylthio]-2-chlorophenyl}-1,1-bis(hydroxymethyl)propyl)acetamide (1023648-29-4)

Guidance literature:

With sodium tetrahydroborate; calcium chloride; In ethanol; water; at 20 ℃;

DOI:10.1016/j.tet.2008.01.086

upstream raw materials:

3-[3-(benzyloxy)phenylthio]-6-vinyl-1-chlorobenzene

2-acetylaminomalonic acid diethyl ester

Downstream raw materials:

N-(3-{4-[3-(benzyloxy)phenylthio]-2-chlorophenyl}-1,1-bis(hydroxymethyl)propyl)acetamide

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