5-methyl-4-phenylhexanenitrile

Base Information

Chemical Name:5-methyl-4-phenylhexanenitrile
CAS No.:107202-86-8
Molecular Formula:C₁₃H₁₇N
Molecular Weight:187.285
Hs Code.:

Synonyms:5-methyl-4-phenylhexanenitrile

Suppliers and Price of 5-methyl-4-phenylhexanenitrile

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 5-methyl-4-phenylhexanenitrile

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 5-methyl-4-phenylhexanenitrile

There total 6 articles about 5-methyl-4-phenylhexanenitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: potassium cyanide

: C₁₉H₂₄O₃S

: 107202-86-8
5-methyl-4-phenylhexanenitrile

Guidance literature:: With potassium iodide; In N,N-dimethyl-formamide; at 60 ℃; for 24h; Inert atmosphere;
DOI:10.1039/c4cc05923a

Reference yield:

: 611-70-1
phenyl isopropyl ketone

: 107202-86-8
5-methyl-4-phenylhexanenitrile

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydride / mineral oil; tetrahydrofuran / 2.08 h / 0 °C / Inert atmosphere

1.2: Inert atmosphere; Reflux

2.1: palladium 10% on activated carbon; hydrogen / methanol / 16 h / 20 °C / 2250.23 - 3000.3 Torr / Inert atmosphere

3.1: lithium aluminium tetrahydride / diethyl ether / 2 h / -40 °C / Inert atmosphere

4.1: pyridine / dichloromethane / 24 h / 20 °C / Inert atmosphere

5.1: potassium iodide / N,N-dimethyl-formamide / 24 h / 60 °C / Inert atmosphere

With pyridine; lithium aluminium tetrahydride; palladium 10% on activated carbon; hydrogen; sodium hydride; potassium iodide; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; N,N-dimethyl-formamide; mineral oil;
DOI:10.1039/c4cc05923a

Reference yield:

: 72277-17-9
(+/-)-ethyl 4-methyl-3-phenylpentanoate

: 107202-86-8
5-methyl-4-phenylhexanenitrile

Guidance literature:: Multi-step reaction with 3 steps

1: lithium aluminium tetrahydride / diethyl ether / 2 h / -40 °C / Inert atmosphere

2: pyridine / dichloromethane / 24 h / 20 °C / Inert atmosphere

3: potassium iodide / N,N-dimethyl-formamide / 24 h / 60 °C / Inert atmosphere

With pyridine; lithium aluminium tetrahydride; potassium iodide; In diethyl ether; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c4cc05923a