2-(2-(benzyloxycarbonylamino)-2-methylpropylsulfonyl)ethanesulfonic acid

Base Information

Chemical Name:2-(2-(benzyloxycarbonylamino)-2-methylpropylsulfonyl)ethanesulfonic acid
CAS No.:1037833-03-6
Molecular Formula:C₁₄H₂₁NO₇S₂
Molecular Weight:379.455
Hs Code.:

Synonyms:2-(2-(benzyloxycarbonylamino)-2-methylpropylsulfonyl)ethanesulfonic acid

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Chemical Property of 2-(2-(benzyloxycarbonylamino)-2-methylpropylsulfonyl)ethanesulfonic acid

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Technology Process of 2-(2-(benzyloxycarbonylamino)-2-methylpropylsulfonyl)ethanesulfonic acid

There total 6 articles about 2-(2-(benzyloxycarbonylamino)-2-methylpropylsulfonyl)ethanesulfonic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.7%

: 1037833-02-5
S-2-(2-(benzyloxycarbonylamino)-2-methylpropylthio)ethyl ethanethioate

: 1032764-16-1
2-(benzyloxycarbonyl)amino-2-methylpropanesulfonic acid

: 1037833-03-6
2-(2-(benzyloxycarbonylamino)-2-methylpropylsulfonyl)ethanesulfonic acid

Guidance literature:: With formic acid; dihydrogen peroxide; In water; at 80 ℃; for 17h;

Reference yield:

: 1037833-02-5
S-2-(2-(benzyloxycarbonylamino)-2-methylpropylthio)ethyl ethanethioate

: 1037833-03-6
2-(2-(benzyloxycarbonylamino)-2-methylpropylsulfonyl)ethanesulfonic acid

Guidance literature:: With formic acid; dihydrogen peroxide; In water; at 25 ℃; for 16h;
DOI:10.1016/j.bmcl.2008.10.114

Reference yield:

: 1037833-01-4
benzyl 1-(2-chloroethylthio)-2-methylpropan-2-ylcarbamate

: 1037833-03-6
2-(2-(benzyloxycarbonylamino)-2-methylpropylsulfonyl)ethanesulfonic acid

Guidance literature:: Multi-step reaction with 2 steps

1: N,N-dimethyl-formamide / 70 °C

2: formic acid; dihydrogen peroxide / water / 17 h / 80 °C

With formic acid; dihydrogen peroxide; In water; N,N-dimethyl-formamide;