C₃₇H₅₂O₆Si

Base Information

Chemical Name:C₃₇H₅₂O₆Si
CAS No.:1320210-76-1
Molecular Formula:C₃₇H₅₂O₆Si
Molecular Weight:620.902
Hs Code.:

C<sub>37</sub>H<sub>52</sub>O<sub>6</sub>Si

Synonyms:C₃₇H₅₂O₆Si

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Chemical Property of C₃₇H₅₂O₆Si

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Technology Process of C₃₇H₅₂O₆Si

There total 10 articles about C₃₇H₅₂O₆Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₄₃H₆₆O₆Si₂

: 1320210-76-1
C₃₇H₅₂O₆Si

Guidance literature:: With methanol; 10-camphorsulfonic acid; at 0 ℃; for 1h; Inert atmosphere;
DOI:10.1016/j.tet.2012.01.071

Reference yield:

: 1320210-69-2
C₂₂H₂₄O₅

: 1320210-76-1
C₃₇H₅₂O₆Si

Guidance literature:: Multi-step reaction with 8 steps

1.1: benzene / 2 h / Inert atmosphere; Reflux

2.1: diisobutylaluminium hydride / hexane; dichloromethane / 0.33 h / -78 °C / Inert atmosphere

3.1: titanium(IV) isopropylate; diethyl (2R,3R)-tartrate / dichloromethane / Inert atmosphere; Molecular sieve

3.2: 10 h / 0 - 20 °C / Inert atmosphere; Molecular sieve

4.1: sodium bis(2-methoxyethoxy)aluminium dihydride / tetrahydrofuran; toluene / 6 h / -40 - 20 °C / Inert atmosphere

4.2: Saturated solution

5.1: sodium hydride / tetrahydrofuran; N,N-dimethyl-formamide / 0 °C / Inert atmosphere

5.2: 19 h / 0 - 60 °C / Inert atmosphere

6.1: methanol; 10-camphorsulfonic acid / 24 h / 20 °C / Inert atmosphere

7.1: 1H-imidazole / N,N-dimethyl-formamide / 2 h / 60 °C / Inert atmosphere

8.1: methanol; 10-camphorsulfonic acid / 1 h / 0 °C / Inert atmosphere

With 1H-imidazole; titanium(IV) isopropylate; methanol; diethyl (2R,3R)-tartrate; sodium hydride; diisobutylaluminium hydride; 10-camphorsulfonic acid; sodium bis(2-methoxyethoxy)aluminium dihydride; In tetrahydrofuran; hexane; dichloromethane; N,N-dimethyl-formamide; toluene; benzene; 1.1: Wittig reaction / 3.1: Sharpless epoxidation / 3.2: Sharpless epoxidation;
DOI:10.1016/j.tet.2012.01.071

Reference yield:

: 1320210-70-5
C₂₅H₂₈O₆

: 1320210-76-1
C₃₇H₅₂O₆Si

Guidance literature:: Multi-step reaction with 7 steps

1.1: diisobutylaluminium hydride / hexane; dichloromethane / 0.33 h / -78 °C / Inert atmosphere

2.1: titanium(IV) isopropylate; diethyl (2R,3R)-tartrate / dichloromethane / Inert atmosphere; Molecular sieve

2.2: 10 h / 0 - 20 °C / Inert atmosphere; Molecular sieve

3.1: sodium bis(2-methoxyethoxy)aluminium dihydride / tetrahydrofuran; toluene / 6 h / -40 - 20 °C / Inert atmosphere

3.2: Saturated solution

4.1: sodium hydride / tetrahydrofuran; N,N-dimethyl-formamide / 0 °C / Inert atmosphere

4.2: 19 h / 0 - 60 °C / Inert atmosphere

5.1: methanol; 10-camphorsulfonic acid / 24 h / 20 °C / Inert atmosphere

6.1: 1H-imidazole / N,N-dimethyl-formamide / 2 h / 60 °C / Inert atmosphere

7.1: methanol; 10-camphorsulfonic acid / 1 h / 0 °C / Inert atmosphere

With 1H-imidazole; titanium(IV) isopropylate; methanol; diethyl (2R,3R)-tartrate; sodium hydride; diisobutylaluminium hydride; 10-camphorsulfonic acid; sodium bis(2-methoxyethoxy)aluminium dihydride; In tetrahydrofuran; hexane; dichloromethane; N,N-dimethyl-formamide; toluene; 2.1: Sharpless epoxidation / 2.2: Sharpless epoxidation;
DOI:10.1016/j.tet.2012.01.071