C₂₃H₃₆O₃

Base Information

• Chemical Name: C₂₃H₃₆O₃
• CAS No.: 1429406-67-6
• Molecular Formula: C₂₃H₃₆O₃
• Molecular Weight: 360.537
• Mol file: 1429406-67-6.mol

Synonyms:C₂₃H₃₆O₃

Chemical Property of C₂₃H₃₆O₃

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of C₂₃H₃₆O₃

There total 3 articles about C₂₃H₃₆O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C9H15I + C22H35BO3 → C23H36O3 (1429406-67-6)

Guidance literature:

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium hydroxide; In tetrahydrofuran; water; at 40 ℃; for 0.5h; Inert atmosphere;

DOI:10.1021/ol400717h

Reference yield:

3-isopropyl-1,2,4-trimethoxy-5-vinylbenzene → C23H36O3 (1429406-67-6)

Guidance literature:

Multi-step reaction with 2 steps

1: tetrahydrofuran / 1 h / 0 - 30 °C / Inert atmosphere

2: sodium hydroxide; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / tetrahydrofuran; water / 0.5 h / 40 °C / Inert atmosphere

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium hydroxide; In tetrahydrofuran; water; 2: |Suzuki-Miyaura Coupling;

DOI:10.1021/ol400717h

Reference yield:

3-(1-methylethyl)-2,4,5-trimethoxybenzaldehyde (144707-41-5) → C23H36O3 (1429406-67-6)

Guidance literature:

Multi-step reaction with 3 steps

1.1: n-butyllithium / hexane; tetrahydrofuran / 2 h / 0 °C / Inert atmosphere

1.2: -78 °C / Inert atmosphere

2.1: tetrahydrofuran / 1 h / 0 - 30 °C / Inert atmosphere

3.1: sodium hydroxide; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / tetrahydrofuran; water / 0.5 h / 40 °C / Inert atmosphere

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; n-butyllithium; sodium hydroxide; In tetrahydrofuran; hexane; water; 3.1: |Suzuki-Miyaura Coupling;

DOI:10.1021/ol400717h

upstream raw materials:

3-(1-methylethyl)-2,4,5-trimethoxybenzaldehyde