C₁₈H₃₁N₃O₂

Base Information

Chemical Name:C₁₈H₃₁N₃O₂
CAS No.:1399318-01-4
Molecular Formula:C₁₈H₃₁N₃O₂
Molecular Weight:321.463
Hs Code.:

C<sub>18</sub>H<sub>31</sub>N<sub>3</sub>O<sub>2</sub>

Synonyms:C₁₈H₃₁N₃O₂

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Chemical Property of C₁₈H₃₁N₃O₂

Chemical Property:

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Technology Process of C₁₈H₃₁N₃O₂

There total 9 articles about C₁₈H₃₁N₃O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₃H₃₉N₃O₄

: 1399318-01-4
C₁₈H₃₁N₃O₂

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 23 ℃; for 1.5h;
DOI:10.1021/jm3008823

Reference yield:

: 27829-72-7
ethyl (E)-hex-2-enoate

: 1399318-01-4
C₁₈H₃₁N₃O₂

Guidance literature:: Multi-step reaction with 9 steps

1: methanesulfonamide; AD-mix α / water; tert-butyl alcohol / 168 h / -1 °C

2: triethylamine / dichloromethane / 24 h / 0 - 23 °C

3: sodium azide / N,N-dimethyl-formamide / 15 h / 23 - 55 °C

4: 10% Pd/C; hydrogen / ethanol / 15 h / 23 °C / Inert atmosphere

5: lithium hydroxide monohydrate / tetrahydrofuran; water / 12 h / 23 °C

6: 1-hydroxybenzotriazol-hydrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 14 h / 23 °C

7: trifluoroacetic acid / dichloromethane / 1.5 h / 23 °C

8: sodium tris(acetoxy)borohydride / dichloromethane / 16 h / 0 - 23 °C

9: trifluoroacetic acid / dichloromethane / 1.5 h / 23 °C

With sodium azide; lithium hydroxide monohydrate; methanesulfonamide; AD-mix α; 10% Pd/C; hydrogen; sodium tris(acetoxy)borohydride; 1-hydroxybenzotriazol-hydrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In tetrahydrofuran; ethanol; dichloromethane; water; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1021/jm3008823

Reference yield:

: 108666-29-1
(2R,3S)-ethyl 2,3-dihydroxyhexanoate

: 1399318-01-4
C₁₈H₃₁N₃O₂

Guidance literature:: Multi-step reaction with 8 steps

1: triethylamine / dichloromethane / 24 h / 0 - 23 °C

2: sodium azide / N,N-dimethyl-formamide / 15 h / 23 - 55 °C

3: 10% Pd/C; hydrogen / ethanol / 15 h / 23 °C / Inert atmosphere

4: lithium hydroxide monohydrate / tetrahydrofuran; water / 12 h / 23 °C

5: 1-hydroxybenzotriazol-hydrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 14 h / 23 °C

6: trifluoroacetic acid / dichloromethane / 1.5 h / 23 °C

7: sodium tris(acetoxy)borohydride / dichloromethane / 16 h / 0 - 23 °C

8: trifluoroacetic acid / dichloromethane / 1.5 h / 23 °C

With sodium azide; lithium hydroxide monohydrate; 10% Pd/C; hydrogen; sodium tris(acetoxy)borohydride; 1-hydroxybenzotriazol-hydrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In tetrahydrofuran; ethanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/jm3008823