C₃₀H₃₉NO₆Si

Base Information

Chemical Name:C₃₀H₃₉NO₆Si
CAS No.:1265279-47-7
Molecular Formula:C₃₀H₃₉NO₆Si
Molecular Weight:537.728
Hs Code.:

C<sub>30</sub>H<sub>39</sub>NO<sub>6</sub>Si

Synonyms:C₃₀H₃₉NO₆Si

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Chemical Property of C₃₀H₃₉NO₆Si

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Technology Process of C₃₀H₃₉NO₆Si

There total 21 articles about C₃₀H₃₉NO₆Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: (2S,4aS,8S,8aR)-8-allyl-8-methyl-3-methylene-1,2,3,4,8,8a-hexahydro-7H-2,4a-ethanonaphthalen-7-one

: 1265279-46-6
C₁₅H₂₁NO₅Si

: 1265279-47-7
C₃₀H₃₉NO₆Si

Guidance literature:: With Hoveyda-Grubbs catalyst second generation; In benzene; at 70 ℃; for 1.17h; Inert atmosphere;
DOI:10.1002/ejoc.201001281

Reference yield:

: 1048970-79-1
C₂₉H₃₄O₃Si

: 1265279-47-7
C₃₀H₃₉NO₆Si

Guidance literature:: Multi-step reaction with 15 steps

1.1: (S)-1-methyl-3,3-diphenyl-hexahydropyrrolo[1,2-c][1,3,2]oxazaborole; benzo[1,3,2]dioxaborole / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere

2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 0 °C / Inert atmosphere

3.1: [bis(acetoxy)iodo]benzene; potassium hydrogencarbonate / 0.5 h / 0 - 23 °C / Inert atmosphere

4.1: Trimethyl borate / toluene / 16.3 h / 23 °C / Inert atmosphere; Reflux

5.1: palladium 10% on activated carbon; hydrogen / methanol / 0.5 h / 23 °C

6.1: pyridinium chlorochromate / dichloromethane / 16 h / 23 °C / Inert atmosphere; Molecular sieve

7.1: potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.5 h / -78 - 0 °C / Inert atmosphere

8.1: bis-triphenylphosphine-palladium(II) chloride; formic acid; tributyl-amine / N,N-dimethyl-formamide / 16 h / 23 - 78 °C / Inert atmosphere

9.1: methanol; samarium diiodide / tetrahydrofuran / 0.33 h / 23 °C / Inert atmosphere

10.1: tetrahydrofuran / 0.5 h / 0 - 23 °C / Inert atmosphere

11.1: tert.-butylhydroperoxide / decane; ethyl acetate / 0.5 h / 23 °C / Inert atmosphere; Molecular sieve

11.2: 16 h / 23 °C / Inert atmosphere

12.1: Martins sulfurane / dichloromethane / 2 h / 23 °C / Inert atmosphere

13.1: N,N,N,N,N,N-hexamethylphosphoric triamide; potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.5 h / -78 °C / Inert atmosphere

13.2: 3 h / -78 - 0 °C / Inert atmosphere

14.1: N,N,N,N,N,N-hexamethylphosphoric triamide; potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.58 h / -78 °C / Inert atmosphere

14.2: 3 h / -78 - 0 °C / Inert atmosphere

15.1: Hoveyda-Grubbs catalyst second generation / benzene / 1.17 h / 70 °C / Inert atmosphere

With methanol; tert.-butylhydroperoxide; N,N,N,N,N,N-hexamethylphosphoric triamide; bis-triphenylphosphine-palladium(II) chloride; formic acid; Hoveyda-Grubbs catalyst second generation; samarium diiodide; Martins sulfurane; Trimethyl borate; tributyl-amine; [bis(acetoxy)iodo]benzene; palladium 10% on activated carbon; tetrabutyl ammonium fluoride; hydrogen; potassium hexamethylsilazane; potassium hydrogencarbonate; pyridinium chlorochromate; (S)-1-methyl-3,3-diphenyl-hexahydropyrrolo[1,2-c][1,3,2]oxazaborole; benzo[1,3,2]dioxaborole; In tetrahydrofuran; methanol; decane; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; toluene; benzene; 1.1: Corey-Bakshi-Shibata reduction / 4.1: Intramolecular Diels-Alder reaction;
DOI:10.1002/ejoc.201001281

Reference yield:

: 108534-61-8
(2-methoxyphenoxy)-(1,1-dimethylethyl)diphenylsilane

: 1265279-47-7
C₃₀H₃₉NO₆Si

Guidance literature:: Multi-step reaction with 16 steps

1.1: N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium / diethyl ether; cyclohexane / 0.75 h / -78 °C / Inert atmosphere

1.2: 2 h / -78 °C / Inert atmosphere

2.1: (S)-1-methyl-3,3-diphenyl-hexahydropyrrolo[1,2-c][1,3,2]oxazaborole; benzo[1,3,2]dioxaborole / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere

3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 0 °C / Inert atmosphere

4.1: [bis(acetoxy)iodo]benzene; potassium hydrogencarbonate / 0.5 h / 0 - 23 °C / Inert atmosphere

5.1: Trimethyl borate / toluene / 16.3 h / 23 °C / Inert atmosphere; Reflux

6.1: palladium 10% on activated carbon; hydrogen / methanol / 0.5 h / 23 °C

7.1: pyridinium chlorochromate / dichloromethane / 16 h / 23 °C / Inert atmosphere; Molecular sieve

8.1: potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.5 h / -78 - 0 °C / Inert atmosphere

9.1: bis-triphenylphosphine-palladium(II) chloride; formic acid; tributyl-amine / N,N-dimethyl-formamide / 16 h / 23 - 78 °C / Inert atmosphere

10.1: methanol; samarium diiodide / tetrahydrofuran / 0.33 h / 23 °C / Inert atmosphere

11.1: tetrahydrofuran / 0.5 h / 0 - 23 °C / Inert atmosphere

12.1: tert.-butylhydroperoxide / decane; ethyl acetate / 0.5 h / 23 °C / Inert atmosphere; Molecular sieve

12.2: 16 h / 23 °C / Inert atmosphere

13.1: Martins sulfurane / dichloromethane / 2 h / 23 °C / Inert atmosphere

14.1: N,N,N,N,N,N-hexamethylphosphoric triamide; potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.5 h / -78 °C / Inert atmosphere

14.2: 3 h / -78 - 0 °C / Inert atmosphere

15.1: N,N,N,N,N,N-hexamethylphosphoric triamide; potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.58 h / -78 °C / Inert atmosphere

15.2: 3 h / -78 - 0 °C / Inert atmosphere

16.1: Hoveyda-Grubbs catalyst second generation / benzene / 1.17 h / 70 °C / Inert atmosphere

With methanol; tert.-butylhydroperoxide; N,N,N,N,N,N-hexamethylphosphoric triamide; bis-triphenylphosphine-palladium(II) chloride; formic acid; Hoveyda-Grubbs catalyst second generation; samarium diiodide; Martins sulfurane; Trimethyl borate; tributyl-amine; N,N,N,N,-tetramethylethylenediamine; [bis(acetoxy)iodo]benzene; palladium 10% on activated carbon; tetrabutyl ammonium fluoride; hydrogen; sec.-butyllithium; potassium hexamethylsilazane; potassium hydrogencarbonate; pyridinium chlorochromate; (S)-1-methyl-3,3-diphenyl-hexahydropyrrolo[1,2-c][1,3,2]oxazaborole; benzo[1,3,2]dioxaborole; In tetrahydrofuran; methanol; diethyl ether; decane; dichloromethane; cyclohexane; ethyl acetate; N,N-dimethyl-formamide; toluene; benzene; 2.1: Corey-Bakshi-Shibata reduction / 5.1: Intramolecular Diels-Alder reaction;
DOI:10.1002/ejoc.201001281