C₂₃H₂₉N₇O₃

Base Information

Chemical Name:C₂₃H₂₉N₇O₃
CAS No.:1228586-33-1
Molecular Formula:C₂₃H₂₉N₇O₃
Molecular Weight:451.528
Hs Code.:

C<sub>23</sub>H<sub>29</sub>N<sub>7</sub>O<sub>3</sub>

Synonyms:C₂₃H₂₉N₇O₃

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Chemical Property of C₂₃H₂₉N₇O₃

Chemical Property:

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Technology Process of C₂₃H₂₉N₇O₃

There total 8 articles about C₂₃H₂₉N₇O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 684220-30-2
4,6-dichloropyrimidine-2-carboxylic acid

: 1228586-33-1
C₂₃H₂₉N₇O₃

Guidance literature:: Multi-step reaction with 6 steps

1: ammonium hydroxide / water; 1-methyl-pyrrolidin-2-one / 4 h / 60 °C

2: N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; 4-methyl-morpholine / N,N-dimethyl-formamide / 60 °C

3: nitric acid; sulfuric acid / water / 45 h / 0 - 23 °C

4: triethylamine / N,N-dimethyl-formamide / 2 h / 23 °C

5: acetic acid; zinc / 3 h / 23 °C

6: manganese(IV) oxide / water; dimethyl sulfoxide / 0.75 h / 80 °C

With 4-methyl-morpholine; manganese(IV) oxide; ammonium hydroxide; sulfuric acid; nitric acid; acetic acid; triethylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; zinc; In 1-methyl-pyrrolidin-2-one; water; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1021/jm400815m

Reference yield:

: 1228587-35-6
C₂₃H₃₁N₇O₂*ClH

: 1228586-33-1
C₂₃H₂₉N₇O₃

Guidance literature:: With manganese(IV) oxide; In water; dimethyl sulfoxide; at 80 ℃; for 0.75h;
DOI:10.1021/jm400815m

Reference yield:

: 1228588-63-3
4-amino-6-chloropyrimidine-2-carboxylic acid

: 1228586-33-1
C₂₃H₂₉N₇O₃

Guidance literature:: Multi-step reaction with 5 steps

1: N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; 4-methyl-morpholine / N,N-dimethyl-formamide / 60 °C

2: nitric acid; sulfuric acid / water / 45 h / 0 - 23 °C

3: triethylamine / N,N-dimethyl-formamide / 2 h / 23 °C

4: acetic acid; zinc / 3 h / 23 °C

5: manganese(IV) oxide / water; dimethyl sulfoxide / 0.75 h / 80 °C

With 4-methyl-morpholine; manganese(IV) oxide; sulfuric acid; nitric acid; acetic acid; triethylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; zinc; In water; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1021/jm400815m