1,1,8,8-tetrakis(5-((benzyloxy)carbonyl)-4-ethyl-3-methylpyrrol-2-yl)octane

Base Information

Chemical Name:1,1,8,8-tetrakis(5-((benzyloxy)carbonyl)-4-ethyl-3-methylpyrrol-2-yl)octane
CAS No.:76367-74-3
Molecular Formula:C₆₈H₇₈N₄O₈
Molecular Weight:1079.39
Hs Code.:

Synonyms:1,1,8,8-tetrakis(5-((benzyloxy)carbonyl)-4-ethyl-3-methylpyrrol-2-yl)octane

Suppliers and Price of 1,1,8,8-tetrakis(5-((benzyloxy)carbonyl)-4-ethyl-3-methylpyrrol-2-yl)octane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,1,8,8-tetrakis(5-((benzyloxy)carbonyl)-4-ethyl-3-methylpyrrol-2-yl)octane

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 1,1,8,8-tetrakis(5-((benzyloxy)carbonyl)-4-ethyl-3-methylpyrrol-2-yl)octane

There total 4 articles about 1,1,8,8-tetrakis(5-((benzyloxy)carbonyl)-4-ethyl-3-methylpyrrol-2-yl)octane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4949-58-0
2-(ethyloxycarbonyl)-3-ethyl-4-methylpyrrole

: 76367-74-3
1,1,8,8-tetrakis(5-((benzyloxy)carbonyl)-4-ethyl-3-methylpyrrol-2-yl)octane

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / base-catalyzed transesterification

2: p-toluenesulfonic acid / benzene / 2 h / Heating

With toluene-4-sulfonic acid; In benzene;
DOI:10.1021/ja00393a007

Reference yield:

: 5012-24-8
5-Ethoxycarbonyl-4-ethyl-3-methylpyrrole-2-carboxylic acid

: 76367-74-3
1,1,8,8-tetrakis(5-((benzyloxy)carbonyl)-4-ethyl-3-methylpyrrol-2-yl)octane

Guidance literature:: Multi-step reaction with 4 steps

1: 95 percent / I₂, NaI, NaHCO₃ / H₂O; 1,2-dichloro-ethane / 1 h / Heating

2: 80 percent / NaI, HCl / ethanol; H₂O / 0.25 h / Heating

3: 95 percent / base-catalyzed transesterification

4: p-toluenesulfonic acid / benzene / 2 h / Heating

With hydrogenchloride; iodine; sodium hydrogencarbonate; toluene-4-sulfonic acid; sodium iodide; In ethanol; water; 1,2-dichloro-ethane; benzene;
DOI:10.1021/ja00393a007

Reference yield:

: 76367-42-5
ethyl 5-carboxy-3-ethyl-5-iodo-4-methylpyrrole-2-carboxylate

: 76367-74-3
1,1,8,8-tetrakis(5-((benzyloxy)carbonyl)-4-ethyl-3-methylpyrrol-2-yl)octane

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / NaI, HCl / ethanol; H₂O / 0.25 h / Heating

2: 95 percent / base-catalyzed transesterification

3: p-toluenesulfonic acid / benzene / 2 h / Heating

With hydrogenchloride; toluene-4-sulfonic acid; sodium iodide; In ethanol; water; benzene;
DOI:10.1021/ja00393a007