2-(trimethylsilyl)ethyl 2,6-di-O-benzoyl-3,4-di-O-levulinoyl-β-D-galactopyranoside

Base Information

Chemical Name:2-(trimethylsilyl)ethyl 2,6-di-O-benzoyl-3,4-di-O-levulinoyl-β-D-galactopyranoside
CAS No.:195323-27-4
Molecular Formula:C₃₅H₄₄O₁₂Si
Molecular Weight:684.813
Hs Code.:

Synonyms:2-(trimethylsilyl)ethyl 2,6-di-O-benzoyl-3,4-di-O-levulinoyl-β-D-galactopyranoside

Suppliers and Price of 2-(trimethylsilyl)ethyl 2,6-di-O-benzoyl-3,4-di-O-levulinoyl-β-D-galactopyranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 2-(trimethylsilyl)ethyl 2,6-di-O-benzoyl-3,4-di-O-levulinoyl-β-D-galactopyranoside

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 2-(trimethylsilyl)ethyl 2,6-di-O-benzoyl-3,4-di-O-levulinoyl-β-D-galactopyranoside

There total 1 articles about 2-(trimethylsilyl)ethyl 2,6-di-O-benzoyl-3,4-di-O-levulinoyl-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 40608-06-8
levulinic anhydride

: 165621-52-3
2-(trimethylsilyl)ethyl 2,6-di-O-benzoyl-β-D-galactopyranoside

: 195323-27-4
2-(trimethylsilyl)ethyl 2,6-di-O-benzoyl-3,4-di-O-levulinoyl-β-D-galactopyranoside

Guidance literature:: With dmap; In pyridine; Ambient temperature;
DOI:10.1080/07328309708006543

Reference yield: 83.0%

: 195323-27-4
2-(trimethylsilyl)ethyl 2,6-di-O-benzoyl-3,4-di-O-levulinoyl-β-D-galactopyranoside

: 2,6-di-O-benzoyl-3,4-di-O-levulinoyl-D-galactopyranoside

Guidance literature:: With trifluoroacetic acid; In dichloromethane; for 4h; Ambient temperature;
DOI:10.1080/07328309708006543

Reference yield:

: 195323-27-4
2-(trimethylsilyl)ethyl 2,6-di-O-benzoyl-3,4-di-O-levulinoyl-β-D-galactopyranoside

: 195323-35-4
2-(tetradecyl)hexadecyl 2,6-di-O-benzoyl-β-D-galactopyranosyl trichloroacetimidate

Guidance literature:: Multi-step reaction with 4 steps

1: 83 percent / TFA / CH₂Cl₂ / 4 h / Ambient temperature

2: 87 percent / Drierite, DBU / CH₂Cl₂ / 2 h / Ambient temperature

3: 75 percent / molecular sieves / CH₂Cl₂ / Ambient temperature

4: 92 percent / hydrazine monoacetate / ethanol / 1.5 h / Ambient temperature

With calcium sulfate; molecular sieve; hydrazinium monoacetate; 1,8-diazabicyclo[5.4.0]undec-7-ene; trifluoroacetic acid; In ethanol; dichloromethane;
DOI:10.1080/07328309708006543