tert-butyl isopropyl[3-nitro-5-(trifluoromethyl)benzyl]carbamate

Base Information

Chemical Name:tert-butyl isopropyl[3-nitro-5-(trifluoromethyl)benzyl]carbamate
CAS No.:1274816-97-5
Molecular Formula:C₁₆H₂₁F₃N₂O₄
Molecular Weight:362.349
Hs Code.:

Synonyms:tert-butyl isopropyl[3-nitro-5-(trifluoromethyl)benzyl]carbamate

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Chemical Property of tert-butyl isopropyl[3-nitro-5-(trifluoromethyl)benzyl]carbamate

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Technology Process of tert-butyl isopropyl[3-nitro-5-(trifluoromethyl)benzyl]carbamate

There total 5 articles about tert-butyl isopropyl[3-nitro-5-(trifluoromethyl)benzyl]carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 1274816-96-4
N-[3-nitro-5-(trifluoromethyl)benzyl]propan-2-amine

: 1274816-97-5
tert-butyl isopropyl[3-nitro-5-(trifluoromethyl)benzyl]carbamate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; at 20 ℃; Cooling with ice;
DOI:10.1021/jm101479y

Reference yield:

: 180146-66-1
(3-nitro-5-(trifluoromethyl)phenyl)methanol

: 1274816-97-5
tert-butyl isopropyl[3-nitro-5-(trifluoromethyl)benzyl]carbamate

Guidance literature:: Multi-step reaction with 3 steps

1: carbon tetrabromide; triphenylphosphine / dichloromethane / 0 - 20 °C

2: dichloromethane / 0 - 20 °C

3: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 20 °C / Cooling with ice

With carbon tetrabromide; N-ethyl-N,N-diisopropylamine; triphenylphosphine; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jm101479y

Reference yield:

: 180146-67-2
1-(bromomethyl)-3-nitro-5-(trifluoromethyl)benzene

: 1274816-97-5
tert-butyl isopropyl[3-nitro-5-(trifluoromethyl)benzyl]carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: dichloromethane / 0 - 20 °C

2: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 20 °C / Cooling with ice

With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jm101479y