5-chloro-1-(1-(3-chlorophenyl)ethyl)-2-imino-1,2-dihydropyridine-3-carboxamide

Base Information

Chemical Name:5-chloro-1-(1-(3-chlorophenyl)ethyl)-2-imino-1,2-dihydropyridine-3-carboxamide
CAS No.:1191907-92-2
Molecular Formula:C₁₄H₁₃Cl₂N₃O
Molecular Weight:310.183
Hs Code.:

Synonyms:5-chloro-1-(1-(3-chlorophenyl)ethyl)-2-imino-1,2-dihydropyridine-3-carboxamide

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Chemical Property of 5-chloro-1-(1-(3-chlorophenyl)ethyl)-2-imino-1,2-dihydropyridine-3-carboxamide

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Technology Process of 5-chloro-1-(1-(3-chlorophenyl)ethyl)-2-imino-1,2-dihydropyridine-3-carboxamide

There total 3 articles about 5-chloro-1-(1-(3-chlorophenyl)ethyl)-2-imino-1,2-dihydropyridine-3-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 6.0%

: 70097-69-7
2-cyano-2-(3,4-dichloro-5-oxo-2,5-dihydrofuran-2-yl)acetamide

: 24358-43-8
1-(3-Chloro-phenyl)-ethylamine

: 1191907-92-2
5-chloro-1-(1-(3-chlorophenyl)ethyl)-2-imino-1,2-dihydropyridine-3-carboxamide

Guidance literature:: 2-cyano-2-(3,4-dichloro-5-oxo-2,5-dihydrofuran-2-yl)acetamide; 1-(3-Chloro-phenyl)-ethylamine; With triethylamine; In tetrahydrofuran; at 20 ℃; for 18h; Cooling with ice;

In water; dimethyl sulfoxide; at 80 ℃; for 1h;
DOI:10.1021/acs.jmedchem.5b01528

Reference yield:

: C₁₅H₁₃Cl₂N₃O₃

: 1191907-92-2
5-chloro-1-(1-(3-chlorophenyl)ethyl)-2-imino-1,2-dihydropyridine-3-carboxamide

Guidance literature:: In water; dimethyl sulfoxide; at 80 ℃; for 1h;

Reference yield:

: 70097-69-7
2-cyano-2-(3,4-dichloro-5-oxo-2,5-dihydrofuran-2-yl)acetamide

: 1191907-92-2
5-chloro-1-(1-(3-chlorophenyl)ethyl)-2-imino-1,2-dihydropyridine-3-carboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / tetrahydrofuran / 20 °C / Cooling with ice

2: water; dimethyl sulfoxide / 1 h / 80 °C

With triethylamine; In tetrahydrofuran; water; dimethyl sulfoxide;