[(S)-2-(2-Methoxymethoxy-ethyl)-1,3-dimethyl-cyclohex-2-enyl]-((S)-2-methoxymethyl-pyrrolidin-1-yl)-methanone

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Chemical Name:[(S)-2-(2-Methoxymethoxy-ethyl)-1,3-dimethyl-cyclohex-2-enyl]-((S)-2-methoxymethyl-pyrrolidin-1-yl)-methanone
CAS No.:179261-06-4
Molecular Formula:C₁₉H₃₃NO₄
Molecular Weight:339.475
Hs Code.:

Synonyms:[(S)-2-(2-Methoxymethoxy-ethyl)-1,3-dimethyl-cyclohex-2-enyl]-((S)-2-methoxymethyl-pyrrolidin-1-yl)-methanone

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Chemical Property of [(S)-2-(2-Methoxymethoxy-ethyl)-1,3-dimethyl-cyclohex-2-enyl]-((S)-2-methoxymethyl-pyrrolidin-1-yl)-methanone

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Technology Process of [(S)-2-(2-Methoxymethoxy-ethyl)-1,3-dimethyl-cyclohex-2-enyl]-((S)-2-methoxymethyl-pyrrolidin-1-yl)-methanone

There total 4 articles about [(S)-2-(2-Methoxymethoxy-ethyl)-1,3-dimethyl-cyclohex-2-enyl]-((S)-2-methoxymethyl-pyrrolidin-1-yl)-methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 179261-05-3
[(S)-2-(2-Methoxymethoxy-ethyl)-1,3-dimethyl-cyclohexa-2,5-dienyl]-((S)-2-methoxymethyl-pyrrolidin-1-yl)-methanone

: 179261-06-4
[(S)-2-(2-Methoxymethoxy-ethyl)-1,3-dimethyl-cyclohex-2-enyl]-((S)-2-methoxymethyl-pyrrolidin-1-yl)-methanone

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethyl acetate; for 72h; Ambient temperature;
DOI:10.1021/jo960568j

Reference yield:

: 63126-47-6
(2S)-2-(methoxymethyl)-1-pyrrolidine

: 179261-06-4
[(S)-2-(2-Methoxymethoxy-ethyl)-1,3-dimethyl-cyclohex-2-enyl]-((S)-2-methoxymethyl-pyrrolidin-1-yl)-methanone

Guidance literature:: Multi-step reaction with 4 steps

1: 86 percent / Et₃N, AlCl₃ / CH₂Cl₂ / 40 h / Ambient temperature

2: 81 percent / N,N-diisopropylethylamine / CH₂Cl₂ / 24 h / Ambient temperature

3: 1.) K, liq. NH₃, t-BuOH, 2.) piperylene / 1.) THF, -78 deg C, 30 min, 2.) -78 deg C, 1 h

4: 95 percent / H₂ / Pd/C / ethyl acetate / 72 h / Ambient temperature

With aluminium trichloride; penta-1,3-diene; ammonia; hydrogen; triethylamine; N-ethyl-N,N-diisopropylamine; tert-butyl alcohol; palladium on activated charcoal; In dichloromethane; ethyl acetate;
DOI:10.1021/jo960568j

Reference yield:

: 179261-16-6
[2-(2-Hydroxy-ethyl)-3-methyl-phenyl]-((S)-2-methoxymethyl-pyrrolidin-1-yl)-methanone

: 179261-06-4
[(S)-2-(2-Methoxymethoxy-ethyl)-1,3-dimethyl-cyclohex-2-enyl]-((S)-2-methoxymethyl-pyrrolidin-1-yl)-methanone

Guidance literature:: Multi-step reaction with 3 steps

1: 81 percent / N,N-diisopropylethylamine / CH₂Cl₂ / 24 h / Ambient temperature

2: 1.) K, liq. NH₃, t-BuOH, 2.) piperylene / 1.) THF, -78 deg C, 30 min, 2.) -78 deg C, 1 h

3: 95 percent / H₂ / Pd/C / ethyl acetate / 72 h / Ambient temperature

With penta-1,3-diene; ammonia; hydrogen; N-ethyl-N,N-diisopropylamine; tert-butyl alcohol; palladium on activated charcoal; In dichloromethane; ethyl acetate;
DOI:10.1021/jo960568j