2,2'-[{5-[(tetrahydro-2H-pyran-2-yloxy)methyl]-1,3-phenylene}bis(oxy)]diethanol

Base Information

Chemical Name:2,2'-[{5-[(tetrahydro-2H-pyran-2-yloxy)methyl]-1,3-phenylene}bis(oxy)]diethanol
CAS No.:1346131-93-8
Molecular Formula:C₁₆H₂₄O₆
Molecular Weight:312.363
Hs Code.:

Synonyms:2,2'-[{5-[(tetrahydro-2H-pyran-2-yloxy)methyl]-1,3-phenylene}bis(oxy)]diethanol

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Chemical Property of 2,2'-[{5-[(tetrahydro-2H-pyran-2-yloxy)methyl]-1,3-phenylene}bis(oxy)]diethanol

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Technology Process of 2,2'-[{5-[(tetrahydro-2H-pyran-2-yloxy)methyl]-1,3-phenylene}bis(oxy)]diethanol

There total 2 articles about 2,2'-[{5-[(tetrahydro-2H-pyran-2-yloxy)methyl]-1,3-phenylene}bis(oxy)]diethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1346131-92-7
tert-butyl(2-{3-(2-{[isopropyl(dimethyl)silyl]oxy}ethoxy)-5-[(tetrahydro-2H-pyran-2-yloxy)methyl]phenoxy}ethoxy)dimethylsilane

: 1346131-93-8
2,2'-[{5-[(tetrahydro-2H-pyran-2-yloxy)methyl]-1,3-phenylene}bis(oxy)]diethanol

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 4h; Inert atmosphere;
DOI:10.1039/c1cc15596b

Reference yield:

: 1346131-91-6
[3,5-bis(2-{[tert-butyl(dimethyl)silyl]oxy}ethoxy)phenyl]methanol

: 1346131-93-8
2,2'-[{5-[(tetrahydro-2H-pyran-2-yloxy)methyl]-1,3-phenylene}bis(oxy)]diethanol

Guidance literature:: Multi-step reaction with 2 steps

1: pyridinium p-toluenesulfonate / dichloromethane / 12 h / 20 °C / Inert atmosphere

2: tetrabutyl ammonium fluoride / tetrahydrofuran / 4 h / 20 °C / Inert atmosphere

With tetrabutyl ammonium fluoride; pyridinium p-toluenesulfonate; In tetrahydrofuran; dichloromethane;
DOI:10.1039/c1cc15596b