3-methoxy-4-(2-methyl-2-((2-(trimethylsilyl)ethoxy)methoxy)propoxy)aniline

Base Information

• Chemical Name: 3-methoxy-4-(2-methyl-2-((2-(trimethylsilyl)ethoxy)methoxy)propoxy)aniline
• CAS No.: 1224171-88-3
• Molecular Formula: C₁₇H₃₁NO₄Si
• Molecular Weight: 341.523

Synonyms:3-methoxy-4-(2-methyl-2-((2-(trimethylsilyl)ethoxy)methoxy)propoxy)aniline

Chemical Property of 3-methoxy-4-(2-methyl-2-((2-(trimethylsilyl)ethoxy)methoxy)propoxy)aniline

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

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Technology Process of 3-methoxy-4-(2-methyl-2-((2-(trimethylsilyl)ethoxy)methoxy)propoxy)aniline

There total 1 articles about 3-methoxy-4-(2-methyl-2-((2-(trimethylsilyl)ethoxy)methoxy)propoxy)aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

(2-((1-(2-methoxy-4-nitrophenoxy)-2-methylpropan-2-yloxy)methoxy)ethyl)trimethylsilane (1224171-87-2) → 3-methoxy-4-(2-methyl-2-((2-(trimethylsilyl)ethoxy)methoxy)propoxy)aniline (1224171-88-3)

Guidance literature:

With hydrogen; palladium 10% on activated carbon; In ethanol; for 4h; under 760.051 Torr;

Reference yield: 100.0%

1-(5-chloropyridin-2-yl)-4-(hydroxymethyl)-1H-pyrazole-3-carboxylic acid (1224172-56-8) + 3-methoxy-4-(2-methyl-2-((2-(trimethylsilyl)ethoxy)methoxy)propoxy)aniline (1224171-88-3) → C27H37ClN4O6Si

Guidance literature:

With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃; for 2h;

DOI:10.1016/j.bmcl.2015.05.008

Reference yield: 61.0%

1-(4-chlorophenyl)-3-(hydroxymethyl)-1H-pyrazole-4-carboxylic acid (1224171-78-1) + 3-methoxy-4-(2-methyl-2-((2-(trimethylsilyl)ethoxy)methoxy)propoxy)aniline (1224171-88-3) → 1-(4-chlorophenyl)-3-(hydroxymethyl)-N-(3-methoxy-4-(2-methyl-2-((2-(trimethylsilyl)ethoxy)methoxy)propoxy)phenyl)-1H-pyrazole-4-carboxamide (1224171-89-4)

Guidance literature:

With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃;

upstream raw materials:

(2-((1-(2-methoxy-4-nitrophenoxy)-2-methylpropan-2-yloxy)methoxy)ethyl)trimethylsilane

Downstream raw materials:

1-(4-chlorophenyl)-3-(hydroxymethyl)-N-(3-methoxy-4-(2-methyl-2-((2-(trimethylsilyl)ethoxy)methoxy)propoxy)phenyl)-1H-pyrazole-4-carboxamide

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