C₁₅H₉⁽²⁾H₅

Base Information

• Chemical Name: C₁₅H₉⁽²⁾H₅
• CAS No.: 877203-67-3
• Molecular Formula: C₁₅H₁₄
• Molecular Weight: 199.236
• Mol file: 877203-67-3.mol

Synonyms:C₁₅H₉⁽²⁾H₅

Chemical Property of C₁₅H₉⁽²⁾H₅

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₅H₉⁽²⁾H₅

There total 1 articles about C₁₅H₉⁽²⁾H₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ethyltriphenylphosphonium bromide (1530-32-1) + 2,3,4,5,6-Pentadeuteriobenzophenon (2694-78-2) → C15H9(2)H5 (877203-67-3)

Guidance literature:

ethyltriphenylphosphonium bromide; With n-butyllithium; In tetrahydrofuran; hexane; at 0 ℃; for 1h;

2,3,4,5,6-Pentadeuteriobenzophenon; In tetrahydrofuran; hexane; at 0 ℃; for 2h;

DOI:10.1021/ja058026j

Reference yield:

C15H9(2)H5 (877203-67-3) → C15H9(2)H5O (877203-68-4)

Guidance literature:

With sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 ℃;

DOI:10.1021/ja058026j

Reference yield:

C15H9(2)H5 (877203-67-3) → C15H9(2)H5O (877203-69-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 0.168 g / mCPBA; NaHCO₃ / CH₂Cl₂ / 0 °C

2: 102 mg / BF₃*OEt₂ / diethyl ether / 0.02 h / 20 °C

With boron trifluoride diethyl etherate; sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; In diethyl ether; dichloromethane;

DOI:10.1021/ja058026j

upstream raw materials:

ethyltriphenylphosphonium bromide

2,3,4,5,6-Pentadeuteriobenzophenon

Downstream raw materials:

C₁₅H₉⁽²⁾H₅O

C₁₅H₉⁽²⁾H₅O

C₁₅H₈⁽²⁾H₅N