methyl 2-hydroxy-5-(2-(N-methylbiphenyl-4-ylsulfonamido)-N-(4-(piperidin-1-yl)benzyl)acetamido)-benzoate

Base Information

Chemical Name:methyl 2-hydroxy-5-(2-(N-methylbiphenyl-4-ylsulfonamido)-N-(4-(piperidin-1-yl)benzyl)acetamido)-benzoate
CAS No.:1456601-93-6
Molecular Formula:C₃₅H₃₇N₃O₆S
Molecular Weight:627.761
Hs Code.:

Synonyms:methyl 2-hydroxy-5-(2-(N-methylbiphenyl-4-ylsulfonamido)-N-(4-(piperidin-1-yl)benzyl)acetamido)-benzoate

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Chemical Property of methyl 2-hydroxy-5-(2-(N-methylbiphenyl-4-ylsulfonamido)-N-(4-(piperidin-1-yl)benzyl)acetamido)-benzoate

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Technology Process of methyl 2-hydroxy-5-(2-(N-methylbiphenyl-4-ylsulfonamido)-N-(4-(piperidin-1-yl)benzyl)acetamido)-benzoate

There total 6 articles about methyl 2-hydroxy-5-(2-(N-methylbiphenyl-4-ylsulfonamido)-N-(4-(piperidin-1-yl)benzyl)acetamido)-benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 1456601-63-0
methyl 2-hydroxy-5-(4-(piperidin-1-yl)benzylamino)benzoate

: 381193-32-4
2-(N-methylbiphenyl-4-ylsulfonamido)acetic acid

: 1456601-93-6
methyl 2-hydroxy-5-(2-(N-methylbiphenyl-4-ylsulfonamido)-N-(4-(piperidin-1-yl)benzyl)acetamido)-benzoate

Guidance literature:: With dichlorotriphenylphosphorane; In dichloromethane; at 80 ℃; for 1h; Inert atmosphere; Microwave irradiation;
DOI:10.1039/c3md20323a

Reference yield: 45.0%

: 1456601-93-6
methyl 2-hydroxy-5-(2-(N-methylbiphenyl-4-ylsulfonamido)-N-(4-(piperidin-1-yl)benzyl)acetamido)-benzoate

Guidance literature:: With dichlorotriphenylphosphorane; In dichloromethane; at 80 ℃; for 1h; Inert atmosphere; Microwave irradiation;

Reference yield:

: 10338-57-5
4-(piperidin-1-yl)benzaldehyde

: 1456601-93-6
methyl 2-hydroxy-5-(2-(N-methylbiphenyl-4-ylsulfonamido)-N-(4-(piperidin-1-yl)benzyl)acetamido)-benzoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: acetic acid / methanol / 1 h / 20 - 40 °C / Molecular sieve

1.2: 2 h / 5 - 20 °C

2.1: dichlorotriphenylphosphorane / dichloromethane / 1 h / 80 °C / Inert atmosphere; Microwave irradiation

With acetic acid; dichlorotriphenylphosphorane; In methanol; dichloromethane;
DOI:10.1039/c3md20323a