2-[5-Chloro-2-(2,4-dichloro-phenoxy)-phenoxy]-propionic acid methoxy carbonyl methyl ester

Base Information

Chemical Name:2-[5-Chloro-2-(2,4-dichloro-phenoxy)-phenoxy]-propionic acid methoxy carbonyl methyl ester
CAS No.:1146530-47-3
Molecular Formula:C₁₈H₁₅Cl₃O₆
Molecular Weight:433.673
Hs Code.:

Synonyms:2-[5-Chloro-2-(2,4-dichloro-phenoxy)-phenoxy]-propionic acid methoxy carbonyl methyl ester

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Chemical Property of 2-[5-Chloro-2-(2,4-dichloro-phenoxy)-phenoxy]-propionic acid methoxy carbonyl methyl ester

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Technology Process of 2-[5-Chloro-2-(2,4-dichloro-phenoxy)-phenoxy]-propionic acid methoxy carbonyl methyl ester

There total 3 articles about 2-[5-Chloro-2-(2,4-dichloro-phenoxy)-phenoxy]-propionic acid methoxy carbonyl methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.6%

: 70006-97-2
2-[5-Chloro-2-(2,4-dichloro-phenoxy)-phenoxy]-propionic acid

: 96-34-4
methyl chloroacetate

: 1146530-47-3
2-[5-Chloro-2-(2,4-dichloro-phenoxy)-phenoxy]-propionic acid methoxy carbonyl methyl ester

Guidance literature:: With triethylamine; In N,N-dimethyl-formamide; at 70 ℃; for 8h;

Reference yield:

: 3380-34-5,88032-08-0
triclosan

: 1146530-47-3
2-[5-Chloro-2-(2,4-dichloro-phenoxy)-phenoxy]-propionic acid methoxy carbonyl methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate; sodium iodide; disodium hydrogenphosphate / acetone / 24 h / Reflux

2.1: sodium hydroxide / 2 h / 90 °C

2.2: 5 °C / pH 2

3.1: triethylamine / N,N-dimethyl-formamide / 8 h / 70 °C

With disodium hydrogenphosphate; potassium carbonate; triethylamine; sodium iodide; sodium hydroxide; In N,N-dimethyl-formamide; acetone;

Reference yield:

: 70006-94-9
2-[5-Chloro-2-(2,4-dichloro-phenoxy)-phenoxy]-propionic acid methyl ester

: 1146530-47-3
2-[5-Chloro-2-(2,4-dichloro-phenoxy)-phenoxy]-propionic acid methoxy carbonyl methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydroxide / 2 h / 90 °C

1.2: 5 °C / pH 2

2.1: triethylamine / N,N-dimethyl-formamide / 8 h / 70 °C

With triethylamine; sodium hydroxide; In N,N-dimethyl-formamide;