2-azidoethyl 2,3,6-tri-O-phenylmethyl-β-D-galactopyranosyl-(1→4)-2,3,6-tri-O-phenylmethyl-β-D-glucopyranoside

Base Information

Chemical Name:2-azidoethyl 2,3,6-tri-O-phenylmethyl-β-D-galactopyranosyl-(1→4)-2,3,6-tri-O-phenylmethyl-β-D-glucopyranoside
CAS No.:914772-38-6
Molecular Formula:C₅₆H₆₁N₃O₁₁
Molecular Weight:952.114
Hs Code.:

Synonyms:2-azidoethyl 2,3,6-tri-O-phenylmethyl-β-D-galactopyranosyl-(1→4)-2,3,6-tri-O-phenylmethyl-β-D-glucopyranoside

Suppliers and Price of 2-azidoethyl 2,3,6-tri-O-phenylmethyl-β-D-galactopyranosyl-(1→4)-2,3,6-tri-O-phenylmethyl-β-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-azidoethyl 2,3,6-tri-O-phenylmethyl-β-D-galactopyranosyl-(1→4)-2,3,6-tri-O-phenylmethyl-β-D-glucopyranoside

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 2-azidoethyl 2,3,6-tri-O-phenylmethyl-β-D-galactopyranosyl-(1→4)-2,3,6-tri-O-phenylmethyl-β-D-glucopyranoside

There total 8 articles about 2-azidoethyl 2,3,6-tri-O-phenylmethyl-β-D-galactopyranosyl-(1→4)-2,3,6-tri-O-phenylmethyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 914772-35-3
(4aR,6S,7R,8S,8aS)-6-[(2R,3R,4S,5R,6R)-6-(2-Azido-ethoxy)-4,5-bis-benzyloxy-2-benzyloxymethyl-tetrahydro-pyran-3-yloxy]-7,8-bis-benzyloxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxine

: 914772-38-6
2-azidoethyl 2,3,6-tri-O-phenylmethyl-β-D-galactopyranosyl-(1→4)-2,3,6-tri-O-phenylmethyl-β-D-glucopyranoside

Guidance literature:: With hydrogenchloride; sodium cyanoborohydride; In tetrahydrofuran; diethyl ether; for 0.5h;
DOI:10.1016/j.tetlet.2006.08.008

Reference yield: 70.9%

: 2-azidoethyl 2,3-di-O-phenylmethyl-4:6-O-phenylmethylene-β-D-galactopyranosyl-(1→4)-2,3,6-tri-O-phenylmethyl-β-D-glucopyranoside

: 914772-38-6
2-azidoethyl 2,3,6-tri-O-phenylmethyl-β-D-galactopyranosyl-(1→4)-2,3,6-tri-O-phenylmethyl-β-D-glucopyranoside

Guidance literature:: 2-azidoethyl 2,3-di-O-phenylmethyl-4:6-O-phenylmethylene-β-D-galactopyranosyl-(1→4)-2,3,6-tri-O-phenylmethyl-β-D-glucopyranoside; With sodium cyanoborohydride; In tetrahydrofuran; at 20 ℃; for 2h; Molecular sieve;

With hydrogenchloride; In tetrahydrofuran; diethyl ether; at 0 - 20 ℃; for 12h; pH=2;
DOI:10.1039/c5ra00759c

Reference yield:

: 230286-11-0
2-azidoethyl β-D-galactopyranosyl-(1->4)-β-D-glucopyranoside

: 914772-38-6
2-azidoethyl 2,3,6-tri-O-phenylmethyl-β-D-galactopyranosyl-(1→4)-2,3,6-tri-O-phenylmethyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: CSA / tetrahydrofuran / 3 h / Heating

2: NaH / dimethylformamide / 20 °C

3: 78 percent / NaCNBH₃; HCl / diethyl ether; tetrahydrofuran / 0.5 h

With hydrogenchloride; camphor-10-sulfonic acid; sodium hydride; sodium cyanoborohydride; In tetrahydrofuran; diethyl ether; N,N-dimethyl-formamide;
DOI:10.1016/j.tetlet.2006.08.008