methyl 2,3-di-O-benzyl-6-O-t-butyldiphenylsilyl-4-deoxy-α-D-glucopyranoside

Base Information

Chemical Name:methyl 2,3-di-O-benzyl-6-O-t-butyldiphenylsilyl-4-deoxy-α-D-glucopyranoside
CAS No.:130798-99-1
Molecular Formula:C₃₇H₄₄O₅Si
Molecular Weight:596.839
Hs Code.:

Synonyms:methyl 2,3-di-O-benzyl-6-O-t-butyldiphenylsilyl-4-deoxy-α-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 2,3-di-O-benzyl-6-O-t-butyldiphenylsilyl-4-deoxy-α-D-glucopyranoside

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Technology Process of methyl 2,3-di-O-benzyl-6-O-t-butyldiphenylsilyl-4-deoxy-α-D-glucopyranoside

There total 5 articles about methyl 2,3-di-O-benzyl-6-O-t-butyldiphenylsilyl-4-deoxy-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: methyl 2,3-di-O-benzyl-6-O-t-butyldiphenylsilyl-4-O-imidazolyl-thiocarbonyl-α-D-glucopyranoside

: 130798-99-1
methyl 2,3-di-O-benzyl-6-O-t-butyldiphenylsilyl-4-deoxy-α-D-glucopyranoside

Guidance literature:: With tri-n-butyl-tin hydride; In toluene; for 12h; Heating;
DOI:10.1016/S0040-4020(01)88025-X

Reference yield:

: 116730-42-8
4,5-bis(benzyloxy)-2-(tert-butyldimethylsilanyloxy)-6-methoxytetrahydropyran-3-ol

: 130798-99-1
methyl 2,3-di-O-benzyl-6-O-t-butyldiphenylsilyl-4-deoxy-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / toluene / Heating

2: 83 percent / nBu₃SnH / toluene / 12 h / Heating

With tri-n-butyl-tin hydride; In toluene;
DOI:10.1016/S0040-4020(01)88025-X

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 130798-99-1
methyl 2,3-di-O-benzyl-6-O-t-butyldiphenylsilyl-4-deoxy-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 99 percent / imidazole / dimethylformamide / 2 h / Ambient temperature

2: 93 percent / toluene / Heating

3: 83 percent / nBu₃SnH / toluene / 12 h / Heating

With 1H-imidazole; tri-n-butyl-tin hydride; In N,N-dimethyl-formamide; toluene;
DOI:10.1016/S0040-4020(01)88025-X