1,7-bis(2-nitrobenzenesulfonyl)-11-fluoro-1,4,7-triazacyclotetradecane

Base Information

• Chemical Name: 1,7-bis(2-nitrobenzenesulfonyl)-11-fluoro-1,4,7-triazacyclotetradecane
• CAS No.: 344950-91-0
• Molecular Formula: C₂₃H₃₀FN₅O₈S₂
• Molecular Weight: 587.65

Synonyms:1,7-bis(2-nitrobenzenesulfonyl)-11-fluoro-1,4,7-triazacyclotetradecane

Chemical Property of 1,7-bis(2-nitrobenzenesulfonyl)-11-fluoro-1,4,7-triazacyclotetradecane

Chemical Property:

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Technology Process of 1,7-bis(2-nitrobenzenesulfonyl)-11-fluoro-1,4,7-triazacyclotetradecane

There total 1 articles about 1,7-bis(2-nitrobenzenesulfonyl)-11-fluoro-1,4,7-triazacyclotetradecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-diethoxyphosphoryl-1,7-bis(2-nitrobenzenesulfonyl)-11-fluoro-1,4,7-triazacyclotetradecane (344950-89-6) → 1,7-bis(2-nitrobenzenesulfonyl)-11-fluoro-1,4,7-triazacyclotetradecane (344950-91-0)

Guidance literature:

With hydrogen bromide; In acetic acid; at 20 ℃; for 22h;

DOI:10.1021/jm901530b

Reference yield: 59.0%

N-[1-methylene-4-(chloromethylene)phenylene]-N-(2-nitrobenzenesulfonyl)-2-(aminomethyl)pyridine (255383-18-7) + 1,7-bis(2-nitrobenzenesulfonyl)-11-fluoro-1,4,7-triazacyclotetradecane (344950-91-0) → N-{4-[1,7-bis(2-nitrobenzenesulfonyl)-11-fluoro-1,4,7-triazacyclotetradecanyl]-1,4-phenylenebis(methylene)}-N-(2-nitrobenzenesulfonyl)-2-(aminomethyl)pyridine (344950-93-2)

Guidance literature:

With potassium carbonate; In acetonitrile; at 80 ℃; for 18h; Inert atmosphere;

DOI:10.1021/jm901530b

upstream raw materials:

4-diethoxyphosphoryl-1,7-bis(2-nitrobenzenesulfonyl)-11-fluoro-1,4,7-triazacyclotetradecane

Downstream raw materials:

N-{4-[1,7-bis(2-nitrobenzenesulfonyl)-11-fluoro-1,4,7-triazacyclotetradecanyl]-1,4-phenylenebis(methylene)}-N-(2-nitrobenzenesulfonyl)-2-(aminomethyl)pyridine

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