methyl 2-(trifluoromethanesulfonyloxy)-5-[2-(trifluoromethanesulfonyloxy)benzoyl]benzoate

Base Information

Chemical Name:methyl 2-(trifluoromethanesulfonyloxy)-5-[2-(trifluoromethanesulfonyloxy)benzoyl]benzoate
CAS No.:1189760-11-9
Molecular Formula:C₁₇H₁₀F₆O₉S₂
Molecular Weight:536.383
Hs Code.:

Synonyms:methyl 2-(trifluoromethanesulfonyloxy)-5-[2-(trifluoromethanesulfonyloxy)benzoyl]benzoate

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Chemical Property of methyl 2-(trifluoromethanesulfonyloxy)-5-[2-(trifluoromethanesulfonyloxy)benzoyl]benzoate

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Technology Process of methyl 2-(trifluoromethanesulfonyloxy)-5-[2-(trifluoromethanesulfonyloxy)benzoyl]benzoate

There total 2 articles about methyl 2-(trifluoromethanesulfonyloxy)-5-[2-(trifluoromethanesulfonyloxy)benzoyl]benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 358-23-6
trifluoromethylsulfonic anhydride

: 2-hydroxy-5-(2-hydroxybenzoyl)benzoic acid methyl ester

: 1189760-11-9
methyl 2-(trifluoromethanesulfonyloxy)-5-[2-(trifluoromethanesulfonyloxy)benzoyl]benzoate

Guidance literature:: 2-hydroxy-5-(2-hydroxybenzoyl)benzoic acid methyl ester; With pyridine; In dichloromethane; at -78 ℃; for 0.166667h;

trifluoromethylsulfonic anhydride; In dichloromethane; at -78 - 0 ℃; for 4h;
DOI:10.1055/s-0029-1217544

Reference yield:

: 17422-74-1
3-Formylchromone

: 1189760-11-9
methyl 2-(trifluoromethanesulfonyloxy)-5-[2-(trifluoromethanesulfonyloxy)benzoyl]benzoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 0 °C / Inert atmosphere

1.2: 12 h / 0 - 20 °C / Inert atmosphere

1.3: Inert atmosphere

2.1: pyridine / dichloromethane / 0.17 h / -78 °C / Inert atmosphere

2.2: 4 h / -78 - 0 °C / Inert atmosphere

With pyridine; trimethylsilyl trifluoromethanesulfonate; In dichloromethane;
DOI:10.1002/ejoc.201100762

Reference yield: 89.0%

: 1189760-11-9
methyl 2-(trifluoromethanesulfonyloxy)-5-[2-(trifluoromethanesulfonyloxy)benzoyl]benzoate

: 213211-69-9
(2-ethoxyphenyl)boronic acid

: 1189760-24-4
methyl 2'-ethoxy-4-[2-(trifluoromethanesulfonyloxy)benzoyl]biphenyl-2-carboxylate

Guidance literature:: With potassium phosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,4-dioxane; at 110 ℃; for 4h;
DOI:10.1055/s-0029-1217544