4-Oxo-pentanoic acid (4aR,6R,7R,8S,8aS)-2-phenyl-6-(2-tetradecyl-hexadecyloxy)-7-((2S,3S,4R,5R,6S)-3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-yloxy)-hexahydro-pyrano[3,2-d][1,3]dioxin-8-yl ester

Base Information

Chemical Name:4-Oxo-pentanoic acid (4aR,6R,7R,8S,8aS)-2-phenyl-6-(2-tetradecyl-hexadecyloxy)-7-((2S,3S,4R,5R,6S)-3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-yloxy)-hexahydro-pyrano[3,2-d][1,3]dioxin-8-yl ester
CAS No.:196204-52-1
Molecular Formula:C₇₅H₁₁₀O₁₂
Molecular Weight:1203.69
Hs Code.:

4-Oxo-pentanoic acid (4aR,6R,7R,8S,8aS)-2-phenyl-6-(2-tetradecyl-hexadecyloxy)-7-((2S,3S,4R,5R,6S)-3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-yloxy)-hexahydro-pyrano[3,2-d][1,3]dioxin-8-yl ester

Synonyms:4-Oxo-pentanoic acid (4aR,6R,7R,8S,8aS)-2-phenyl-6-(2-tetradecyl-hexadecyloxy)-7-((2S,3S,4R,5R,6S)-3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-yloxy)-hexahydro-pyrano[3,2-d][1,3]dioxin-8-yl ester

Suppliers and Price of 4-Oxo-pentanoic acid (4aR,6R,7R,8S,8aS)-2-phenyl-6-(2-tetradecyl-hexadecyloxy)-7-((2S,3S,4R,5R,6S)-3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-yloxy)-hexahydro-pyrano[3,2-d][1,3]dioxin-8-yl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-Oxo-pentanoic acid (4aR,6R,7R,8S,8aS)-2-phenyl-6-(2-tetradecyl-hexadecyloxy)-7-((2S,3S,4R,5R,6S)-3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-yloxy)-hexahydro-pyrano[3,2-d][1,3]dioxin-8-yl ester

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 4-Oxo-pentanoic acid (4aR,6R,7R,8S,8aS)-2-phenyl-6-(2-tetradecyl-hexadecyloxy)-7-((2S,3S,4R,5R,6S)-3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-yloxy)-hexahydro-pyrano[3,2-d][1,3]dioxin-8-yl ester

There total 4 articles about 4-Oxo-pentanoic acid (4aR,6R,7R,8S,8aS)-2-phenyl-6-(2-tetradecyl-hexadecyloxy)-7-((2S,3S,4R,5R,6S)-3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-yloxy)-hexahydro-pyrano[3,2-d][1,3]dioxin-8-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 2,3,4-tri-O-benzyl-1-deoxy-1-thio-α-L-fucopyranose

: 196204-51-0
4-Oxo-pentanoic acid (4aR,6R,7R,8R,8aS)-7-hydroxy-2-phenyl-6-(2-tetradecyl-hexadecyloxy)-hexahydro-pyrano[3,2-d][1,3]dioxin-8-yl ester

: 196204-52-1
4-Oxo-pentanoic acid (4aR,6R,7R,8S,8aS)-2-phenyl-6-(2-tetradecyl-hexadecyloxy)-7-((2S,3S,4R,5R,6S)-3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-yloxy)-hexahydro-pyrano[3,2-d][1,3]dioxin-8-yl ester

Guidance literature:: With N-iodo-succinimide; methanesulfonic acid; In toluene; at -20 ℃; for 1h;
DOI:10.1271/bbb.61.1615

Reference yield:

: 1125-88-8
benzaldehyde dimethyl acetal

: 196204-52-1
4-Oxo-pentanoic acid (4aR,6R,7R,8S,8aS)-2-phenyl-6-(2-tetradecyl-hexadecyloxy)-7-((2S,3S,4R,5R,6S)-3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-yloxy)-hexahydro-pyrano[3,2-d][1,3]dioxin-8-yl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 78 percent / 10-camphorsulfonic acid / dimethylformamide / 0.75 h / 45 °C

2: 93 percent / DMAP / pyridine / 1 h / -50 °C

3: 89 percent / N-iodosiccinimide, MesOH, 4A MS / toluene / 1 h / -20 °C

With dmap; N-iodo-succinimide; methanesulfonic acid; (1S)-10-camphorsulfonic acid; In pyridine; N,N-dimethyl-formamide; toluene;
DOI:10.1271/bbb.61.1615

Reference yield:

: 171733-54-3
2-(tetradecyl)hexadecyl β-D-galactopyranoside

: 196204-52-1
4-Oxo-pentanoic acid (4aR,6R,7R,8S,8aS)-2-phenyl-6-(2-tetradecyl-hexadecyloxy)-7-((2S,3S,4R,5R,6S)-3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-yloxy)-hexahydro-pyrano[3,2-d][1,3]dioxin-8-yl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 78 percent / 10-camphorsulfonic acid / dimethylformamide / 0.75 h / 45 °C

2: 93 percent / DMAP / pyridine / 1 h / -50 °C

3: 89 percent / N-iodosiccinimide, MesOH, 4A MS / toluene / 1 h / -20 °C

With dmap; N-iodo-succinimide; methanesulfonic acid; (1S)-10-camphorsulfonic acid; In pyridine; N,N-dimethyl-formamide; toluene;
DOI:10.1271/bbb.61.1615