N-(p-toluenesulfonyl)pyrrolo diazene

Base Information

Chemical Name:N-(p-toluenesulfonyl)pyrrolo diazene
CAS No.:152940-78-8
Molecular Formula:C₁₃H₁₃N₃O₂S
Molecular Weight:275.331
Hs Code.:

Synonyms:N-(p-toluenesulfonyl)pyrrolo diazene

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Chemical Property of N-(p-toluenesulfonyl)pyrrolo diazene

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Technology Process of N-(p-toluenesulfonyl)pyrrolo diazene

There total 6 articles about N-(p-toluenesulfonyl)pyrrolo diazene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 41969-71-5
diethyl pyrrole-3,4-dicarboxylate

: 152940-78-8
N-(p-toluenesulfonyl)pyrrolo diazene

Guidance literature:: Multi-step reaction with 6 steps

1: 91 percent / Bu₄NHSO₄, KOH / CH₂Cl₂

2: 91 percent / DIBAL / CH₂Cl₂

3: 78 percent / Ph₃PCl₂ / CH₂Cl₂

4: 87 percent / NaH / dimethylsulfoxide

5: HCl / diethyl ether

6: dimethyl azodicarboxylate

With hydrogenchloride; potassium hydroxide; tetra(n-butyl)ammonium hydrogensulfate; dichlorotriphenyl-λ⁴-phosphane; sodium hydride; diisobutylaluminium hydride; dimethyl azodicarboxylate; In diethyl ether; dichloromethane; dimethyl sulfoxide;
DOI:10.1021/ja963113k

Reference yield:

: 152940-73-3
3,4-Bis(chloromethyl)-N-tosylpyrrole

: 152940-78-8
N-(p-toluenesulfonyl)pyrrolo diazene

Guidance literature:: Multi-step reaction with 3 steps

1: 87 percent / NaH / dimethylsulfoxide

2: HCl / diethyl ether

3: dimethyl azodicarboxylate

With hydrogenchloride; sodium hydride; dimethyl azodicarboxylate; In diethyl ether; dimethyl sulfoxide;
DOI:10.1021/ja963113k

Reference yield:

: 152940-72-2
N-p-toluenesulfonylpyrrole-3,4-dimethanol

: 152940-78-8
N-(p-toluenesulfonyl)pyrrolo diazene

Guidance literature:: Multi-step reaction with 4 steps

1: 78 percent / Ph₃PCl₂ / CH₂Cl₂

2: 87 percent / NaH / dimethylsulfoxide

3: HCl / diethyl ether

4: dimethyl azodicarboxylate

With hydrogenchloride; dichlorotriphenyl-λ⁴-phosphane; sodium hydride; dimethyl azodicarboxylate; In diethyl ether; dichloromethane; dimethyl sulfoxide;
DOI:10.1021/ja963113k