2-aminomethyl-4-methoxyphenyl iodide

Base Information

Chemical Name:2-aminomethyl-4-methoxyphenyl iodide
CAS No.:1189788-15-5
Molecular Formula:C₈H₁₀INO
Molecular Weight:263.078
Hs Code.:

Synonyms:2-aminomethyl-4-methoxyphenyl iodide

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Chemical Property of 2-aminomethyl-4-methoxyphenyl iodide

Chemical Property:

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Technology Process of 2-aminomethyl-4-methoxyphenyl iodide

There total 3 articles about 2-aminomethyl-4-methoxyphenyl iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 1189788-39-3
C₈H₈IN₃O

: 1189788-15-5
2-aminomethyl-4-methoxyphenyl iodide

Guidance literature:: With triphenylphosphine; In tetrahydrofuran; water; at 20 ℃; for 15h;
DOI:10.1021/jm900476c

Reference yield: 45.0%

: 77287-58-2
2-iodo-5-methoxybenzaldehyde

: 1189788-15-5
2-aminomethyl-4-methoxyphenyl iodide

Guidance literature:: With tetrachlorosilane; sodium iodide; In 1,2-dichloro-ethane; acetonitrile; at 20 ℃; for 48h;
DOI:10.1055/s-0031-1290899

Reference yield:

: 591-31-1
3-methoxy-benzaldehyde

: 1189788-15-5
2-aminomethyl-4-methoxyphenyl iodide

Guidance literature:: Multi-step reaction with 2 steps

1: sulfuric acid; iodine; periodic acid / water; acetic acid / 24 h / 70 °C

2: tetrachlorosilane; sodium iodide / 1,2-dichloro-ethane; acetonitrile / 48 h / 20 °C

With tetrachlorosilane; sulfuric acid; iodine; periodic acid; sodium iodide; In water; acetic acid; 1,2-dichloro-ethane; acetonitrile;
DOI:10.1055/s-0031-1290899