5-{(1E,3Z)-3-[benzyl(oxido)imino]prop-1-en-1-yl}-2-(4-chlorophenyl)-2H-tetrazole

Base Information

• Chemical Name: 5-{(1E,3Z)-3-[benzyl(oxido)imino]prop-1-en-1-yl}-2-(4-chlorophenyl)-2H-tetrazole
• CAS No.: 802910-92-5
• Molecular Formula: C₁₇H₁₄ClN₅O
• Molecular Weight: 339.784

Synonyms:5-{(1E,3Z)-3-[benzyl(oxido)imino]prop-1-en-1-yl}-2-(4-chlorophenyl)-2H-tetrazole

Chemical Property of 5-{(1E,3Z)-3-[benzyl(oxido)imino]prop-1-en-1-yl}-2-(4-chlorophenyl)-2H-tetrazole

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Technology Process of 5-{(1E,3Z)-3-[benzyl(oxido)imino]prop-1-en-1-yl}-2-(4-chlorophenyl)-2H-tetrazole

There total 1 articles about 5-{(1E,3Z)-3-[benzyl(oxido)imino]prop-1-en-1-yl}-2-(4-chlorophenyl)-2H-tetrazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

N-benzyl hydroxylalmine (622-30-0) + 2-(4-chlorophenyl)-5-[(1E)-3-oxoprop-1-en-1-yl]-2H-tetrazole (670276-69-4) → 5-{(1E,3Z)-3-[benzyl(oxido)imino]prop-1-en-1-yl}-2-(4-chlorophenyl)-2H-tetrazole (802910-92-5)

Guidance literature:

With sodium sulfate; In dichloromethane; at 20 ℃; for 0.416667h;

DOI:10.3987/com-04-10158

Reference yield: 48.0%

anthranilic acid (118-92-3,159201-01-1,50816-84-7,80206-34-4,104809-47-4) + 5-{(1E,3Z)-3-[benzyl(oxido)imino]prop-1-en-1-yl}-2-(4-chlorophenyl)-2H-tetrazole (802910-92-5) → 2-benzyl-3-{(E)-2-[2-(4-chlorophenyl)-2H-tetrazol-5-yl]vinyl}-2,3-dihydro-1,2-benzisoxazole

Guidance literature:

anthranilic acid; With isopentyl nitrite; trichloroacetic acid; In tetrahydrofuran; at 18 - 25 ℃; for 1h;

5-{(1E,3Z)-3-[benzyl(oxido)imino]prop-1-en-1-yl}-2-(4-chlorophenyl)-2H-tetrazole; In tetrahydrofuran; for 2h; Heating;

DOI:10.3987/com-04-10158

Reference yield: 35.0%

N-methylmaleimide (930-88-1) + 5-{(1E,3Z)-3-[benzyl(oxido)imino]prop-1-en-1-yl}-2-(4-chlorophenyl)-2H-tetrazole (802910-92-5) → (3S,3aS,6aR)-2-benzyl-3-{(E)-2-[2-(4-chlorophenyl)-2H-tetrazol-5-yl]vinyl}-5-methyldihydro-2H-pyrrolo[3,4-d]isoxazole-4,6(3H,5H)-dione + (3R,3aS,6aR)-2-benzyl-3-{(E)-2-[2-(4-chlorophenyl)-2H-tetrazol-5-yl]vinyl}-5-methyldihydro-2H-pyrrolo[3,4-d]isoxazole-4,6(3H,5H)-dione

Guidance literature:

In toluene; for 20.5h; Heating;

DOI:10.3987/com-04-10158

upstream raw materials:

N-benzyl hydroxylalmine

2-(4-chlorophenyl)-5-[(1E)-3-oxoprop-1-en-1-yl]-2H-tetrazole

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